Effect of Different Nano-Fillers Addition on The Mechanical Properties of Heat-Polymerized Acrylic Resin

Mohamed Aboshama, Aly Sayed, Ahmed Elhagali
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引用次数: 1

Abstract

Aim: To evaluate flexural strength (FS) and micro-hardness of poly(methylmethacrylate) (PMMA) denture base material modified with Zirconium oxide (ZrO2), titanium oxide (TiO2) and zinc oxide (ZnO) nanoparticles powder with different concentration (1.5, 3 and 5% ) Subjects and Methods: Test specimens of PMMA of dimensions (65 ×10 × 2.5 mm) were made from heat-cured acrylic resin served as control group Another nine group were made of PMMA containing 1.5, 3, and 5% (w/w) (ZrO2), (TiO2) and (ZnO) nanoparticles. Two types of mechanical tests were performed on the samples: flexural strength and hardness. Results: Statistical analysis results revealed that non-significant increase in flexural strength of heat cured reinforced with ZrO2 Nps and ZnO Nps for all concentrations. While adding 1.5% and 5% of TiO2 Nps showed significant increase in flexural strength but 3% showed significant decrease values. Results revealed that non-significant decrease in hardness of heat cured reinforced with ZrO2 Nps ,TiO2 Nps, and ZnO Nps for all concentrations except 3% of heat cured reinforced with TiO2 Nps which showed non-significant increase in hardness. Conclusions: It was discovered that adding of 1.5and 5% Tio2 Nps to the used denture base materials would improve the flexural strength of the denture base materials. Also, adding 1.5, 3 and 5 % ZrO2, Tio2, and ZnO Nps reduces the microhardness. of its merits this material has many applications including biomedical and dental prostheses. The main disadvantages of PMMA are its low strength characteristics, which include flexural and impact strengths. (1) Nanotechnology has lately been utilized in the prosthetics scope to material boost objectives (2,3) , which has been confirmed in the research of nanomaterials for enhancing the mechanical characteristics
不同纳米填料对热聚合丙烯酸树脂力学性能的影响
目的:研究不同浓度(1.5、3、5%)氧化锆(ZrO2)、氧化钛(TiO2)和氧化锌(ZnO)纳米粉体改性聚甲基丙烯酸甲酯(PMMA)义齿基托材料的抗弯强度(FS)和显微硬度。采用热固化丙烯酸树脂制成尺寸为(65 ×10 × 2.5 mm)的PMMA试样作为对照组。另外9组分别由含有1.5、3、5% (w/w) (ZrO2)、(TiO2)和(ZnO)纳米粒子的PMMA制成。对样品进行了两种类型的力学测试:弯曲强度和硬度。结果:统计分析结果显示,ZrO2 Nps和ZnO Nps在所有浓度下对热固化增强材料的抗弯强度均无显著提高。添加1.5%和5%的TiO2 Nps显著提高了材料的抗弯强度,添加3%的TiO2 Nps显著降低了材料的抗弯强度。结果表明,除3%的TiO2 Nps增强材料硬度无显著升高外,其余三种浓度的ZrO2 Nps、TiO2 Nps和ZnO Nps增强材料的硬度均无显著降低。结论:发现在使用过的义齿基托材料中添加1.5和5% Tio2 Nps可以提高义齿基托材料的抗弯强度。此外,添加1.5%、3%和5%的ZrO2、Tio2和ZnO Nps可以降低显微硬度。由于其优点,这种材料有许多应用,包括生物医学和牙科修复。PMMA的主要缺点是它的低强度特性,包括弯曲和冲击强度。(1)近年来,纳米技术已被广泛应用于假肢领域,用于材料提升目标(2,3),这在纳米材料增强机械特性的研究中得到了证实
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