CHARACTERISATION OF EPOXY NANOCOMPOSITES REINFORCED BY POTASSIUM TITANATE WHISKER

Wan-Ting Sun, H. Takagi, A. N. Nakagaito
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Abstract

The mechanical and physical properties of potassium titanate whisker (PTW) reinforced epoxy nanocomposites have been studied to examine the contribution of PTW loading and surface modification effects on these properties. Tensile tests and micro-hardness measurements have been used to study the mechanical performance of epoxy-based nanocomposites reinforced with 1 wt% to 5 wt% of PTW. We found that the mechanical properties and micro-hardness of PTW-reinforced epoxy nanocomposites become higher than those of neat epoxy resin. Furthermore, the experimental results showed that the nanocomposites reinforced with silane-treated PTW have higher tensile strength and Young’s modulus. The micro-hardness of the treated PTW nanocomposites also had higher values as compared with that of untreated PTW nanocomposites. These results indicate that the mechanical performances of the PTW/epoxy nanocomposites were controlled by the silane surface treatment. Scanning electron microscopy studies indicated that the fracture surface of the silane-treated PTW nanocomposite had better interfacial adhesion, as the PTWs were covered with matrix resin.
钛酸钾晶须增强环氧纳米复合材料的表征
研究了钛酸钾晶须(PTW)增强环氧纳米复合材料的力学和物理性能,考察了PTW载荷和表面改性对这些性能的影响。通过拉伸试验和显微硬度测试,研究了添加1 ~ 5 wt% PTW的环氧基纳米复合材料的力学性能。结果表明,ptw增强环氧纳米复合材料的力学性能和显微硬度均高于纯环氧树脂。此外,实验结果表明,硅烷处理的PTW增强纳米复合材料具有更高的抗拉强度和杨氏模量。处理后的PTW纳米复合材料的显微硬度也高于未处理的PTW纳米复合材料。这些结果表明,硅烷表面处理控制了PTW/环氧纳米复合材料的力学性能。扫描电镜研究表明,硅烷处理的PTW纳米复合材料的断口表面覆盖了基体树脂,具有较好的界面附着力。
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