Obtaining and studying the properties of cobalt- and nickel-containing nanocomposites by thermolysis, using saturated carboxylates as precedors

R. V. Saprykin, S. Semenov
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引用次数: 0

Abstract

Nickel (II) and cobalt (II) salts were synthesized with saturated monocarboxylic acids: butyric, valeric, nylon,enanthic, and caprylic. The obtained compounds were characterized by elemental analysis, IR spectroscopy,and differential scanning calorimetry. As a result of thermolysis of the synthesized carboxylates, nanocomposites were obtained, which were studied by scanning and transmission electron microscopy, elemental analysis, IR spectroscopy, energy dispersive X-ray spectroscopy, and X-ray phase analysis. The magnetic properties of the obtained nanocomposites have been studied.
以饱和羧酸盐为前驱体,通过热裂解法制备含钴、含镍纳米复合材料,并对其性能进行了研究
镍(II)和钴(II)盐是用饱和的单羧酸:丁酸、戊酸、尼龙酸、烯酸和辛酸合成的。用元素分析、红外光谱和差示扫描量热法对所得化合物进行了表征。对合成的羧酸盐进行热裂解得到纳米复合材料,并通过扫描电镜、透射电镜、元素分析、红外光谱、能量色散x射线光谱和x射线物相分析对其进行了研究。对制备的纳米复合材料的磁性能进行了研究。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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