Pemisahan Butanol dari Campuran ABE Menggunakan Software Aspen Plus: Pengaruh Refluks Rasio terhadap Kandungan Butanol

D. Nury, Pramahadi Febriyanto, Lisa Anggraini Ismi, Rahmat Taufik Hidayah
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Abstract

Production of acetone-butanol-ethanol (ABE) through the fermentation process is one alternative that needs to be developed. Less economical in the ABE fermentation process is the difficulty of the separation process from the fermentation product and the by-products of the reaction. Among the separation process methods, such as extraction, distillation, adsorption, and gas stripping, the distillation method is still the most widely used method in the ABE separation process. The purpose of this study was to provide recommendations for predicting good ABE separation and producing optimum operating conditions to produce high % butanol content. Which is then simulated using Aspen Plus V11 software. This study varied the reflux ratio in the distillation column and the decanter operating temperature. The results showed that butanol purity reached 90.33% in the radfrac 1 column operated at a pressure of 1.3 atm with a reflux ratio of 5, the location of the 7th feed stage and the number of stages 11. Then proceed to the purification stage in the radfrac column 2 which is operated at a pressure of 2 atm with a reflux ratio of 5, the location of the 4th stage feed and the number of stages 5. The decrease in the reflux ratio of the radfrac column causes a decrease in the butanol content at the bottom so that the purity of butanol also decreases and decreases % recovery or recovery of butanol. This is also followed by the location of the feed stage, which is getting higher, and the number of stages is increasing.
通过发酵工艺生产丙酮-丁醇-乙醇(ABE)是一种需要开发的替代方法。ABE发酵过程中较不经济的是发酵产物和反应副产物的分离过程的困难。在萃取、精馏、吸附、气提等分离工艺方法中,精馏法仍是ABE分离工艺中应用最广泛的方法。本研究的目的是为预测良好的ABE分离和生产高%丁醇含量的最佳操作条件提供建议。然后使用Aspen Plus V11软件进行模拟。本研究改变了精馏塔回流比和卧螺器操作温度。结果表明,radfrac 1塔在压力为1.3 atm、回流比为5、第7进料段位置为7级、段数为11级的条件下,丁醇纯度可达90.33%。然后进入radfrac塔2的净化阶段,在2atm的压力下操作,回流比为5,第4级进料的位置和5级的数量。radfrac塔回流比的降低导致底部丁醇含量的降低,使丁醇纯度也随之降低,使丁醇的回收率或回收率降低。其次是进料级的位置越来越高,进料级的数量也越来越多。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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