The Effect of in-situ Formation of Al2O3 or Fe3AlC on the Structural and Mechanical Properties of FeAl Intermetallic Alloys

K. Isonishi, M. Hashii, K. Ameyama
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引用次数: 6

Abstract

The effect of in-situ formation of reinforcing phase on the mechanical properties of FeAl intermetallic alloy was studied. The in-situ FeAl composites containing Al2O3 or Fe3AlC were fabricated by mechanical alloying of elemental powders and mill scale powder followed by vacuum hot pressing. The starting materials were mixed in the appropriate ratio to synthesize 10vol% of the reinforcing phase. FeAl+Al2O3 and FeAl+Fe3AlC alloys showed high hardness value of HV813 and HV524, respectively. The effect of testing temperature on the 0.2% proof stress was evaluated at the temperature range from room to 1273K under compression. FeAl+Al2O3 and FeAl+Fe3AlC alloy showed proof stress of 2240MPa and 1380MPa at room temperature, respectively. At higher temperatures above 773K the proof stress decreased rapidly. The FeAl base in-situ composites including Fe3AlC or Al2O3 showed the high stress exponent and activation energy in the temperatures range of 1073-1273K.
原位生成Al2O3或Fe3AlC对FeAl金属间合金组织和力学性能的影响
研究了原位形成增强相对FeAl金属间合金力学性能的影响。采用机械合金化方法,将单质粉末与磨屑粉末进行机械合金化,然后进行真空热压,制备了含Al2O3或Fe3AlC的原位FeAl复合材料。将原料按适当比例混合,合成10vol%的增强相。FeAl+Al2O3和FeAl+Fe3AlC合金的硬度值分别为HV813和HV524。在室温至1273K的压缩温度范围内,评估了测试温度对0.2%抗压应力的影响。FeAl+Al2O3和FeAl+Fe3AlC合金在室温下的抗应力分别为2240MPa和1380MPa。在773K以上的高温下,抗压应力迅速下降。含Fe3AlC和Al2O3的FeAl基原位复合材料在1073 ~ 1273k温度范围内表现出较高的应力指数和活化能。
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