Microscopic observation and analysis of field electron emission sites by using an Electron Emission Microscope and Auger Electron Spectrometer

T. Kanai, Y. Yamano, S. Kobayashi, Y. Saito
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Abstract

Field electron emission is recognized as one of important phenomena related to the occurrence of electrical breakdown in vacuum. In this paper, we investigated the distribution of field electron emission sites on a plane electrode before and after current conditioning procedure. The investigation was carried out by scanning the electrode to measure the emission current flowing through the pin-hole of the objective lens of Electron Emission Microscope. As a result, before current conditioning localized emission sites were found. Those emission sites and the current from the sites were unstable in the early stage of high voltage application. During current conditioning and electrode scanning, some of emission sites disappeared, while the others continued to flow current. Sometimes new emission sites appeared at the other points on the electrode surface. After the investigation of emission sites distribution, microscopic observation on some of emission sites were carried out by using the Electron Emission Microscope. Electron emission microscope enables simultaneous observations of field electron emission image and photo electron emission image. The observation revealed that field electron emission occurred at the foreign particles on the electrode surface, and only some of them became electron emission sites. To characterize the emission sites, we observed the absorption current image and analyzed the chemical composition of the emission sites by using an Auger Electron Spectrometer. Observation and analysis suggest that the foreign particle was a semiconducting or insulating material composed of carbon.
利用电子发射显微镜和俄歇电子能谱仪对场电子发射部位进行了显微观察和分析
场电子发射是真空中发生电击穿的重要现象之一。本文研究了电流调节前后平面电极上场电子发射位的分布。采用扫描电极测量电子发射显微镜物镜针孔内的发射电流的方法进行了研究。结果,在电流调节之前,发现了局部排放位点。在高压应用初期,这些发射点及其产生的电流是不稳定的。在电流调节和电极扫描过程中,一些发射位点消失,而其他发射位点继续流动。有时在电极表面的其他点上出现新的发射位点。在对发射点分布进行调查后,利用电子发射显微镜对部分发射点进行了显微观察。电子发射显微镜可以同时观察场电子发射图像和光电子发射图像。观察发现,在电极表面的外来粒子发生场电子发射,只有一部分成为电子发射位点。为了表征发射点,我们观察了吸收电流图像,并用俄歇电子能谱仪分析了发射点的化学成分。观察和分析表明,外来颗粒是由碳组成的半导体或绝缘材料。
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