Recrystallization Experiments in Tensile Deformed 〈100〉- and 〈111〉-Oriented Copper Single Crystals

U. Klement, F. Ernst, P. Wilbrandt
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引用次数: 2

Abstract

〈100〉- and 〈111〉-oriented copper single crystals were tensile deformed to a final strain of 20% and 4%, respectively. Specimens prepared from these crystals were abraded at one end. During the subsequent annealing treatment (750 K, 2 h for the 〈100〉-oriented crystals and 750 K, 90 min for the 〈111〉-oriented crystals) the recrystallization process started on this side. In both cases the orientation relationships between the largest recrystallized grains and the uniformly oriented deformed microstructure can be characterized by the following relations: 22.6° 〈100〉, 21.8° 〈111〉, 46.8° 〈111〉 and 129.8° 〈540〉. Additionally, in the 〈111〉 crystals other orientation relationships were found. This is caused by the different dislocation densities in the specimens. The 〈111〉-oriented crystals represent the early stage of recrystallization whereas the 〈100〉-oriented crystals show the orientations of the late recrystallization stage. Between these stages a further selection of orientations occur.
拉伸变形< 100 >和< 111 >取向铜单晶的再结晶实验
< 100 >和< 111 >取向铜单晶分别拉伸至最终应变的20%和4%。用这些晶体制备的标本一端被磨碎。在随后的退火处理(< 100 >取向晶体750 K, 2 h, < 111 >取向晶体750 K, 90 min)中,再结晶过程从这一侧开始。在这两种情况下,最大再结晶晶粒与均匀取向变形组织的取向关系可表征为:22.6°< 100 >、21.8°< 111 >、46.8°< 111 >和129.8°< 540 >。此外,在< 111 >晶体中发现了其他取向关系。这是由于试样中位错密度不同造成的。< 111 >取向晶体为早期再结晶阶段,< 100 >取向晶体为后期再结晶阶段。在这两个阶段之间,发生了进一步的定向选择。
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