Fabrication of Size-Tunable Silica Particles During Seed-Growth Process

M. Jarzębski, T. Śliwa, Małgorzata Jarzębska, K. Szutkowski
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引用次数: 3

Abstract

Abstract The size control is one of the most important factors during seed-growth process. Although precise determination of ingredients concentrations is easily controllable during the growth process, there is still a possibility to synthesize oversized particles. Nanosized fluorescent silica particles were synthetized using Stöber process and verified using three complementary methods of particle size determination, namely Dynamic Light Scattering (DLS), Particle Tracking (PT) as well as by Transmission Electron Microscopy (TEM) and Confocal Microscopy. The final diameter was verified by DLS and estimated to 494 nm. Parameters necessary to control the size were derived.
在种子生长过程中制备尺寸可调的二氧化硅颗粒
摘要种子大小控制是种子生长过程中最重要的因素之一。虽然在生长过程中很容易控制成分浓度的精确测定,但仍有可能合成超大颗粒。采用Stöber工艺合成纳米二氧化硅荧光粒子,并采用动态光散射(DLS)、粒子跟踪(PT)以及透射电子显微镜(TEM)和共聚焦显微镜三种互补的粒径测定方法对纳米二氧化硅荧光粒子进行了验证。最终直径经DLS验证,估计为494 nm。导出了控制尺寸所需的参数。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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