Friction stir processing to improve grain refinement and superplasticity of Al-Mg-Mn-Cr alloy

A. Kishchik, Ahmed O. Mosleh, O. Yakovtseva, A. Kotov, A. Mikhaylovskaya
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Abstract

Abstract. In this study the Al-4.8Mg-1.0Mn-0.15Cr alloy was frictionally stir processed in order to enhance grain refinement effect and superplastic properties. The microstructure after friction stir processing (FSP) was analyzed using light, scanning and transmission electron microscopies. An additional cold rolling (50%) was performed after the FSP, and a comparative study in terms of microstructure and superplasticity was done between the samples processed using hot rolling and further FSP, FSP and cold rolling, and cold rolling without FSP. The superplastic properties were studied at temperatures of 450 and 500 °C with constant strain rates of 1×10-2 and 1×10-2 s-1. The treatment regime including FSP and further cold rolling improved superplasticity due to fine-grained and homogeneous grain structure with a good thermal stability. At a temperature of 500°C and strain rates of 1×10-3 - 1×10-2 s-1 the alloy demonstrated 330-450 % elongation with a flow stress of 10-20 MPa.
搅拌摩擦处理改善Al-Mg-Mn-Cr合金的晶粒细化和超塑性
摘要本研究对Al-4.8Mg-1.0Mn-0.15Cr合金进行摩擦搅拌处理,以提高晶粒细化效果和超塑性性能。采用光镜、扫描电镜和透射电镜对搅拌摩擦处理(FSP)后的微观结构进行了分析。在FSP后进行额外的冷轧(50%),并对热轧和进一步FSP、FSP和冷轧以及不进行FSP的冷轧试样的组织和超塑性进行了比较研究。在温度为450℃和500℃,应变速率为1×10-2和1×10-2 s-1的条件下,研究了材料的超塑性性能。经FSP和进一步冷轧处理后,由于晶粒细且均匀,具有良好的热稳定性,提高了超塑性。当温度为500℃,应变速率为1×10-3 ~ 1×10-2 s-1时,合金的延伸率为330 ~ 450%,流动应力为10 ~ 20 MPa。
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