I. I. Lestari, D. U. C. Rahayu, D. A. Nurani, Y. Krisnandi, E. Budianto
{"title":"Ethylenediamine-derived imidazoline synthesis using MAOS (Microwave Assisted Organic Synthesis) method","authors":"I. I. Lestari, D. U. C. Rahayu, D. A. Nurani, Y. Krisnandi, E. Budianto","doi":"10.1063/1.5132493","DOIUrl":null,"url":null,"abstract":"In searching of an alternative organic compound for corrosion inhibitor, ethylenediamine-derived imidazoline was successfully synthesized by reacting ethylenediamine (EDA) with stearic acid (SA) using MAOS (Microwave Assisted Organic Synthesis) method with various reaction times. The optimum yield of EDA-SA imidazoline was 94.3 % at 5 min reaction time. EDA-SA imidazoline was identified using TLC and melting point analyzer. Moreover, the structure of EDA-SA imidazoline had been elucidated using UV-Vis, FTIR, 1H-NMR, and LC-MS/MS spectral data. This study revealed that ethylenediamine-derived imidazoline can be synthesized using MAOS method which can be used as a corrosion inhibitor towards carbon steel as further application.In searching of an alternative organic compound for corrosion inhibitor, ethylenediamine-derived imidazoline was successfully synthesized by reacting ethylenediamine (EDA) with stearic acid (SA) using MAOS (Microwave Assisted Organic Synthesis) method with various reaction times. The optimum yield of EDA-SA imidazoline was 94.3 % at 5 min reaction time. EDA-SA imidazoline was identified using TLC and melting point analyzer. Moreover, the structure of EDA-SA imidazoline had been elucidated using UV-Vis, FTIR, 1H-NMR, and LC-MS/MS spectral data. This study revealed that ethylenediamine-derived imidazoline can be synthesized using MAOS method which can be used as a corrosion inhibitor towards carbon steel as further application.","PeriodicalId":376274,"journal":{"name":"PROCEEDINGS OF THE 4TH INTERNATIONAL SYMPOSIUM ON CURRENT PROGRESS IN MATHEMATICS AND SCIENCES (ISCPMS2018)","volume":"30 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2019-11-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"3","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"PROCEEDINGS OF THE 4TH INTERNATIONAL SYMPOSIUM ON CURRENT PROGRESS IN MATHEMATICS AND SCIENCES (ISCPMS2018)","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1063/1.5132493","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 3
Abstract
In searching of an alternative organic compound for corrosion inhibitor, ethylenediamine-derived imidazoline was successfully synthesized by reacting ethylenediamine (EDA) with stearic acid (SA) using MAOS (Microwave Assisted Organic Synthesis) method with various reaction times. The optimum yield of EDA-SA imidazoline was 94.3 % at 5 min reaction time. EDA-SA imidazoline was identified using TLC and melting point analyzer. Moreover, the structure of EDA-SA imidazoline had been elucidated using UV-Vis, FTIR, 1H-NMR, and LC-MS/MS spectral data. This study revealed that ethylenediamine-derived imidazoline can be synthesized using MAOS method which can be used as a corrosion inhibitor towards carbon steel as further application.In searching of an alternative organic compound for corrosion inhibitor, ethylenediamine-derived imidazoline was successfully synthesized by reacting ethylenediamine (EDA) with stearic acid (SA) using MAOS (Microwave Assisted Organic Synthesis) method with various reaction times. The optimum yield of EDA-SA imidazoline was 94.3 % at 5 min reaction time. EDA-SA imidazoline was identified using TLC and melting point analyzer. Moreover, the structure of EDA-SA imidazoline had been elucidated using UV-Vis, FTIR, 1H-NMR, and LC-MS/MS spectral data. This study revealed that ethylenediamine-derived imidazoline can be synthesized using MAOS method which can be used as a corrosion inhibitor towards carbon steel as further application.