Synthesis and CO gas adsorption properties of GO/ZnFe2O4 nanocomposites

Vinh Thanh Nguyen, Tuan Quoc Tran, Cuong Van Nguyen, Hung Van Nguyen, Hai Thanh Nguyen, Hang Thi Bui, Dang Van Tran, Quy Van Nguyen
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Abstract

In this work, ZnFe2O4 nanoparticles were synthesized by hydrothermal method while the hummer method was used to synthesize GO nanosheet. GO/ZnFe2O4 nanocomposites (GO/ZFO) were prepared by mixing of GO with ZnFe2O4 in mass ratio of 1:99, respectively. The structure, morphology, and physical – chemical characteristics were determined by Raman spectroscopy, Transform Electron Microscopy (TEM), and Fourier Transform Infrared Spectroscopy (FT-IR). The CO gas adsorption properties of GO/ZFO were investigated in the range of 25 – 200 ppm at room temperature using quartz crystal microbalance (QCM). GO/ZFO nanocomposites show great adsorption – desorption capacity, high repeatability, and the largest adsorption performance of 1.21‰ (0.098 µg.cm-2 at 200 ppm). The results show that this new approach is promising of spinel structure materials for CO adsorption at room temperature. 
GO/ZnFe2O4纳米复合材料的合成及其CO气体吸附性能
本文采用水热法合成纳米ZnFe2O4,蜂鸟法合成氧化石墨烯纳米片。将氧化石墨烯与ZnFe2O4以1:99的质量比混合制备了氧化石墨烯/ZnFe2O4纳米复合材料(GO/ZFO)。采用拉曼光谱(Raman spectroscopy, TEM)和傅里叶红外光谱(Fourier Transform Infrared spectroscopy, FT-IR)对其结构、形貌和理化性质进行了表征。采用石英晶体微天平(QCM)研究了常温下氧化石墨烯/氧化锆在25 ~ 200 ppm范围内对CO气体的吸附性能。GO/ZFO纳米复合材料具有良好的吸附-解吸能力,重复性高,最大吸附性能为1.21‰(0.098µg)。Cm-2 (200ppm)。结果表明,该方法是一种很有前途的用于室温CO吸附的尖晶石结构材料。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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