Alaa F. Hashim Al- Ajeeli, Khalid. H. Razeg, Ibrahim Fuad Tariq
{"title":"Copper At Silica Core - Shell Nanoparticles As Antibacterial Agents By Sol-Gel Chemical Methods","authors":"Alaa F. Hashim Al- Ajeeli, Khalid. H. Razeg, Ibrahim Fuad Tariq","doi":"10.17993/3ctecno.2023.v12n1e43.337-352","DOIUrl":null,"url":null,"abstract":"Core-shell Cu@sio2 nanoparticles were created by a chemical reaction in a sol gel, and their ability to inhibit S. aureus and E. coli bacteria was tested, when synthesized and characterized using ultraviolet-visible spectroscopy, a copper band could be seen before and after encapsulation at wavelengths of 625 nanometers and 635 nanometers, which are surface plasmonic resonant frequency bands, respectively. The production of Cu @Sio2 core shell nanoparticles was further confirmed using field emission scanning electron microscope (FESEM) pictures. The core shell nanoparticles have a mean size of 66 nanometers and a spherical shape, as shown in TEM. The X-ray diffraction patterns for the nanoparticles, which show face-centered cubic (FCC) of copper, match the crystal structure of Cu@sio2 we discovered using fourier transform infrared (FT-IR) spectroscopy, the fourier transform infrared interaction between the silica and the synthesized copper NPs was investigated. This revealed the capping of the CuNPs by SiO2. The inhibition zone was evident as a result of the activities of these compounds (14, 14, 16, and 20) and (24, 24, 28, and 30) against Escherichia coli bacteria and Staphylococcus aureus bacteria, respectively.","PeriodicalId":210685,"journal":{"name":"3C Tecnología_Glosas de innovación aplicadas a la pyme","volume":"37 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2023-03-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"3C Tecnología_Glosas de innovación aplicadas a la pyme","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.17993/3ctecno.2023.v12n1e43.337-352","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
Abstract
Core-shell Cu@sio2 nanoparticles were created by a chemical reaction in a sol gel, and their ability to inhibit S. aureus and E. coli bacteria was tested, when synthesized and characterized using ultraviolet-visible spectroscopy, a copper band could be seen before and after encapsulation at wavelengths of 625 nanometers and 635 nanometers, which are surface plasmonic resonant frequency bands, respectively. The production of Cu @Sio2 core shell nanoparticles was further confirmed using field emission scanning electron microscope (FESEM) pictures. The core shell nanoparticles have a mean size of 66 nanometers and a spherical shape, as shown in TEM. The X-ray diffraction patterns for the nanoparticles, which show face-centered cubic (FCC) of copper, match the crystal structure of Cu@sio2 we discovered using fourier transform infrared (FT-IR) spectroscopy, the fourier transform infrared interaction between the silica and the synthesized copper NPs was investigated. This revealed the capping of the CuNPs by SiO2. The inhibition zone was evident as a result of the activities of these compounds (14, 14, 16, and 20) and (24, 24, 28, and 30) against Escherichia coli bacteria and Staphylococcus aureus bacteria, respectively.