Eutectic Al2O3–GdAlO3 composite consolidated by combined rapid quenching and spark plasma sintering technique

Young-Hwan Han, M. Nagata, N. Uekawa, K. Kakegawa
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引用次数: 37

Abstract

Abstract A mixture of Al2O3 and GdAlO3 was melted and rapid quenched to produce an amorphous film. Dense eutectic composites were consolidated from ground amorphous powder using both conventional and spark plasma sintering (SPS). Conventional sintering at temperatures above 1600°C for 24 h was required for complete sintering. However, using SPS complete sintering could be obtained at temperatures between 1300 and 1500°C with no soaking. The SPS technique could consolidate ultrafine eutectic structure from rapid quenched amorphous material, whilst conventional sintering was not successful owing to grain growth. A combination of rapid quenching and SPS resulted in an ultrafine eutectic Al2O3–GdAlO3 structure.
采用快速淬火和火花等离子烧结相结合的方法巩固共晶Al2O3-GdAlO3复合材料
摘要将Al2O3和GdAlO3的混合物熔化并快速淬火,得到非晶薄膜。采用传统等离子烧结和放电等离子烧结两种方法,对非晶粉末进行了致密共晶复合材料的固结。要完全烧结,需要在1600℃以上的温度下进行24小时的常规烧结。然而,使用SPS可以在1300 ~ 1500℃的温度下获得完全烧结,而无需浸泡。SPS技术可以在快速淬火的非晶材料中巩固超细共晶组织,而传统烧结由于晶粒长大而不能成功。快速淬火和SPS共同作用形成了Al2O3-GdAlO3超细共晶结构。
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