{"title":"Perbandingan Komponen Aktif Minyak Atsiri dari Daging Buah Pala Kering Cabinet Dryer Melalui Metode Distilasi Air dan Air-Uap","authors":"S. G. Sipahelut","doi":"10.30598/jagritekno.2019.8.1.8","DOIUrl":null,"url":null,"abstract":"The demand for essential oils has increased recently due to the growing of parfume, cosmetic, pharacentical, food and beverage, natural flavourings, medicines, aroma therapy, as well as non-food industries. Nutmeg fruit flesh is one of the potential sources of essential oils which can be obtained by both water distilation and water-steam distillation. Gas Chromatography-Mass Spectometry (GC-MS) is a dynamic analytical method to separate and to detect volatile compounds in a mixture. This study was aimed to compare active components of essential oils from cabinet dryer-dried nutmeg fruit flesh by water distillation and water-steam distillation. Results showed that 28 compounds were detected in essential oils of nutmeg flesh by water distillation, while 31 were identified in oil by water-steam distillation. Compounds identified with higher intensity in oil by water distillation were α-pinene (15.8%), β-pinene (12.0%), limonene (7.5%), δ-terpinene (8.7%), terpinene-4 -ol (14.4%), α-terpineol (4.9%), and myristicin (15.6%). The similar compounds were also detected in oil by water-steam distillation but in different quantities such as 13,3%, 8,8%, 7,2%, 8,7%, 15,6%, 7,7%, 13,5%, respectively. \nKeywords: distillation method, essential oil component, GC-MS, nutmeg fruit flesh \n \nABSTRAK \nPerkembangan industri parfum, kosmetik, farmasi, makanan dan minuman, penyedap alami, obat-obatan, aroma terapi, maupun industri bukan makanan semakin tahun semakin meningkat yang berakibat meningkatnya kebutuhan minyak atsiri. Daging buah pala menjadi salah satu potensi sumber minyak atsiri yang dapat diperoleh melalui metode distilasi (distilasi air dan distilasi air-uap). Kromatografi Gas Spectrometer Massa (GC-MS) merupakan metode yang dinamis untuk pemisahan dan deteksi senyawa-senyawa yang mudah menguap dalam suatu campuran. Tujuan penelitian ini adalah membandingkan komponen senyawa aktif minyak atsiri dari daging buah pala kering cabinet dryer yang diperoleh dari distilasi air dan distilasi air-uap menggunakan GC-MS. Hasil analisis GC-MS minyak atsiri daging buah pala yang diperoleh melalui distilasi air terdapat 28 senyawa, sedangkan dengan distilasi air-uap diperoleh 31 senyawa. Intensitas tertinggi pada metode distilasi air teridentifikasi sebagai senyawa α-pinene (15,8%), β-pinene (12,0%), limonene (7,5%), δ-terpinene (8,7%), Terpinene-4-ol (14,4%), α-terpineol (4,9%), dan myristicin (15,6%), sedangkan intensitas tertinggi pada metode distilasi air-uap teridentifikasi sebagai senyawa α-pinene (13,3%), β-pinene (8,8%), Limonene (7,2%), δ-terpinene (8,7%), terpinene-4-ol (15,6%), α-terpineol (7,7%), dan myristicin (13,5%). \nKata kunci: daging buah pala, GC-MS, komponen minyak atsiri, metode distilasi","PeriodicalId":114215,"journal":{"name":"AGRITEKNO, Jurnal Teknologi Pertanian","volume":"73 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2019-09-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"5","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"AGRITEKNO, Jurnal Teknologi Pertanian","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.30598/jagritekno.2019.8.1.8","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 5
Abstract
The demand for essential oils has increased recently due to the growing of parfume, cosmetic, pharacentical, food and beverage, natural flavourings, medicines, aroma therapy, as well as non-food industries. Nutmeg fruit flesh is one of the potential sources of essential oils which can be obtained by both water distilation and water-steam distillation. Gas Chromatography-Mass Spectometry (GC-MS) is a dynamic analytical method to separate and to detect volatile compounds in a mixture. This study was aimed to compare active components of essential oils from cabinet dryer-dried nutmeg fruit flesh by water distillation and water-steam distillation. Results showed that 28 compounds were detected in essential oils of nutmeg flesh by water distillation, while 31 were identified in oil by water-steam distillation. Compounds identified with higher intensity in oil by water distillation were α-pinene (15.8%), β-pinene (12.0%), limonene (7.5%), δ-terpinene (8.7%), terpinene-4 -ol (14.4%), α-terpineol (4.9%), and myristicin (15.6%). The similar compounds were also detected in oil by water-steam distillation but in different quantities such as 13,3%, 8,8%, 7,2%, 8,7%, 15,6%, 7,7%, 13,5%, respectively.
Keywords: distillation method, essential oil component, GC-MS, nutmeg fruit flesh
ABSTRAK
Perkembangan industri parfum, kosmetik, farmasi, makanan dan minuman, penyedap alami, obat-obatan, aroma terapi, maupun industri bukan makanan semakin tahun semakin meningkat yang berakibat meningkatnya kebutuhan minyak atsiri. Daging buah pala menjadi salah satu potensi sumber minyak atsiri yang dapat diperoleh melalui metode distilasi (distilasi air dan distilasi air-uap). Kromatografi Gas Spectrometer Massa (GC-MS) merupakan metode yang dinamis untuk pemisahan dan deteksi senyawa-senyawa yang mudah menguap dalam suatu campuran. Tujuan penelitian ini adalah membandingkan komponen senyawa aktif minyak atsiri dari daging buah pala kering cabinet dryer yang diperoleh dari distilasi air dan distilasi air-uap menggunakan GC-MS. Hasil analisis GC-MS minyak atsiri daging buah pala yang diperoleh melalui distilasi air terdapat 28 senyawa, sedangkan dengan distilasi air-uap diperoleh 31 senyawa. Intensitas tertinggi pada metode distilasi air teridentifikasi sebagai senyawa α-pinene (15,8%), β-pinene (12,0%), limonene (7,5%), δ-terpinene (8,7%), Terpinene-4-ol (14,4%), α-terpineol (4,9%), dan myristicin (15,6%), sedangkan intensitas tertinggi pada metode distilasi air-uap teridentifikasi sebagai senyawa α-pinene (13,3%), β-pinene (8,8%), Limonene (7,2%), δ-terpinene (8,7%), terpinene-4-ol (15,6%), α-terpineol (7,7%), dan myristicin (13,5%).
Kata kunci: daging buah pala, GC-MS, komponen minyak atsiri, metode distilasi
由于香水、化妆品、制药、食品和饮料、天然香料、药物、芳香疗法以及非食品行业的增长,对精油的需求最近有所增加。肉豆蔻果肉是肉豆蔻精油的潜在来源之一,可通过水蒸馏法和水蒸气蒸馏法提取。气相色谱-质谱联用是一种分离和检测混合物中挥发性化合物的动态分析方法。本研究旨在比较柜式干燥肉豆蔻果肉水蒸馏法和水蒸汽蒸馏法提取的有效成分。结果表明,水蒸馏法从肉豆蔻精油中检出28种化合物,水蒸汽蒸馏法从肉豆蔻精油中检出31种化合物。通过水蒸馏法在油品中鉴定出强度较高的化合物依次为α-蒎烯(15.8%)、β-蒎烯(12.0%)、柠檬烯(7.5%)、δ-松油烯(8.7%)、松油烯-4 -醇(14.4%)、α-松油醇(4.9%)和肉豆素(15.6%)。水-蒸汽蒸馏法在油中也检测到类似的化合物,但含量不同,分别为13、3%、8、8%、7、2%、8、7%、15、6%、7、7%、13、5%。Perkembangan industrii parm, kosmetik, farmasi, makanan dan minuman, penyedap alami, obat-obatan, aroma terapi, maupun industrii bukan makanan semakin tahun semakin meningkat yang berakibat meningkatya kebutuhan minyak atsiri。大庆buah pala menjadi salah satu potentisi sumer minyak atsiri yang dapat diperoleh melalui metode distilasi(蒸馏空气)。气相色谱-质谱联用仪(GC-MS):测定阳阳峰、阳阳峰、阳阳峰、阳阳峰和阳阳峰。图juan penelitian ini adalah成员,kan komponen senyawa aktif minyak atsiri dari dagingbuah palkering cabinet干燥机yang diperoleh dari distilasi air蒸馏器空气蒸馏器menggunakan气相色谱-质谱联用。采用气相色谱-质谱联用分析方法,测定了四川芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山芦山。Intensitas tertingi pada metode distilasi air teridentifii sebagai senyawa α-蒎烯(15.8%)、β-蒎烯(12.0%)、柠檬烯(7.5%)、δ-松油烯(8.7%)、松油烯-4-醇(14.4%)、α-松油醇(4.9%)、丹肉豆蔻素(15.6%)、sedangkan Intensitas tertingi pada metode distilasi air- up teridentifikasi sebagai senyawa α-蒎烯(13.3%)、β-蒎烯(8.8%)、柠檬烯(7.2%)、δ-松油烯(8.7%)、松油烯-4-醇(15.6%)、α-松油醇(7.7%)、丹肉豆蔻素(13.5%)。Kata kunci:大黄酒,气相色谱-质谱分析,komponen minyak atsiri, metode distilasi