A Nature Based Solution: Production and Characterization of Biomass Derived Catalyst from Nigerian Baobab Fruit Shell Powder (Adansonia Digitata).

Eze Ji, Nwaeze Ia
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Abstract

Work on biomass synthesized catalyst from Nigerian Baobab fruit shell powder was thermally treated at 550o C for 6 hours using a muffle furnace. The resultant calcined powder and the un-calcined were characterized using Fourier Transform Infrared spectroscopy (FTIR), Scanning Electron Microscopy (SEM) and X-ray Diffraction (XRD) and further compared with the un-calcined form (baobab fruit shell powder). The FTIR revealed the presence of functional groups matched as alkenes with carbon-hydrogen and nitrogen-hydrogen bonds for baobab fruit shell powder (BFSP). With C-O, a carbon stretch at 1118 & 670 cm-1 and C-H alkyne for the biomass derived catalyst (BDC) from baobab. The morphology of the samples using SEM indicated the presence of higher porosity in the calcined sample when compared to the uncalcined. The superimposed graph of intensity vs 2 theta, of the BFSP and BDC showed no crystallinity during phase determination causing differing diffraction peak counts with no width from 200 – 450 , characteristic to biomass of plant or animal origin. Related outcome was seen for XRD results.
基于自然的解决方案:尼日利亚猴面包树果壳粉生物质衍生催化剂的生产和表征。
以尼日利亚猴面包树果壳粉为原料,采用马弗炉在550℃下加热6小时制备生物质合成催化剂。利用傅里叶变换红外光谱(FTIR)、扫描电镜(SEM)和x射线衍射(XRD)对煅烧后的粉末和未煅烧后的粉末进行了表征,并与未煅烧后的粉末(猴面包树果壳粉)进行了比较。FTIR结果表明,猴面包树果壳粉(BFSP)中存在碳氢键和氮氢键匹配的烯烃官能团。以猴面包树为原料的生物质衍生催化剂(BDC)含有碳氧化合物(C-O)和碳链(C-H炔),碳链长度为1118和670 cm-1。利用扫描电镜对样品进行形貌分析,发现煅烧后的样品孔隙率高于未煅烧的样品。BFSP和BDC的强度与2 θ的叠加图显示,在相测定过程中没有结晶度,导致衍射峰计数不同,宽度在200 - 450之间,这是植物或动物来源生物量的特征。XRD结果也有相关结果。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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