Discoloration of flowable and universal resin composites immersed in black tea for 30 days

Ayaka Hori-Ishikawa, Y. Ogawa, Ayako Okada, Nana Sakaeda, Daichi Aizawa, M. Hanabusa, K. Ohmori, Takatsugu Yamamoto
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Abstract

Purpose: This study evaluated the discoloration of current flowable and universal resin composites by immersing in black tea over 30 days. Materials and Methods: Three flowable resin composites and three universal resin composites were evaluated. The composites were inserted into a disk-shaped stainless steel mold and properly cured. The surfaces of the composite disks were wet-ground and ultrasonically cleaned. Colors – L*, a*, and b* were measured at the center of disks on a gray background using a spectrophotometer. The disks were immersed in black tea at 37 ̊C for 30 days, and the colors were repeatedly measured at 1, 3, 5, and 30 days of immersion. Color differences ΔE*ab were calculated from the L*, a*, and b* values. Water sorption and solubility of the composites were also measured as per ISO 4049. The results were statistically analyzed, and regression analyses were done between ΔE*ab and ΔL*, Δa*, Δb* or sorption/solubility. Results: All the composites showed observable increases of ΔE*ab within the first 5 days of immersion. Values of ΔE*ab ranged from 0.64 to 4.97, and three composites exhibited values above the clinically acceptable value, 3.3. ΔL* and Δb* revealed strong correlations with ΔE*ab. Both water sorption and solubility had positive correlations with ΔE*ab at 30 days. Conclusion: Tea immersion induced discoloration of the current resin composites. This discoloration was affected most by the change in brightness and difference in its blue-yellow chromaticity, and the level of discoloration was material dependent. (Asian Pac J Dent 2020; 20: 9-15.)
可流动和通用树脂复合材料浸泡在红茶中30天的变色
目的:研究通用树脂复合材料在红茶中浸泡30天后的变色情况。材料与方法:对三种可流动树脂复合材料和三种通用树脂复合材料进行了评价。将复合材料插入圆盘形不锈钢模具中并进行适当固化。对复合圆盘表面进行湿磨和超声清洗。用分光光度计在灰色背景上的圆盘中心测量L*、a*和b*三种颜色。将这些圆盘浸泡在37℃的红茶中30天,并在浸泡1、3、5和30天时反复测量颜色。色差ΔE*ab根据L*, a*和b*值计算。根据ISO 4049测试了复合材料的吸水性和溶解度。对结果进行统计分析,并对ΔE*ab与ΔL*、Δa*、Δb*或吸附/溶解度进行回归分析。结果:所有复合材料在浸泡前5天内ΔE*ab均有明显升高。ΔE*ab的取值范围为0.64 ~ 4.97,其中3个组合值高于临床可接受值3.3。ΔL*和Δb*与ΔE*ab有很强的相关性。30 d时吸水性和溶解度均与ΔE*ab呈正相关。结论:茶浸可引起树脂复合材料的变色。这种变色受其亮度变化和蓝黄色度差异的影响最大,变色程度与材料有关。(亚太学报2020;20: 15)。
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