Influence of different stabilizers to the growth of ZnO nanostructures on TiO2 seed layer

N. Asib, K. A. Juhaizat, M. H. Mamat, M. Rusop, Z. Khusaimi
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引用次数: 1

Abstract

In this work, zinc oxide (ZnO) nanostructures prepared by immersion method with zinc nitrate hexahydrate (Zn(NO3)2.6H2O) as a precursor were successfully grown on TiO2 seed layer with three different stabilizers i.e. hexamethylenetetramine, C6H12N4 (HMTA), urea (CH4N2O) and sodium hydroxide (NaOH). The effect of various stabilizers on the size particles, surface morphologies and element composition in grown ZnO were investigated by using ZETA nanoparticle sizer, FESEM and EDX. Size particles of ZnO solutions after immersion method was observed and the smallest particles sizes were recorded for HMTA. FESEM images showed that ZnO nanorods, nanoflowers and grain-like structures were formed when using HMTA, urea and NaOH as stabilizer. The presence of ZnO and TiO2 were confirmed by EDX analysis by showing that all samples that used stabilizer have highest weight % of Zn element.
不同稳定剂对TiO2种子层ZnO纳米结构生长的影响
本文以六水硝酸锌(Zn(NO3)2.6H2O)为前驱体,采用浸渍法制备了氧化锌纳米结构,并在TiO2种子层上成功生长了三种不同的稳定剂:六亚甲基四胺、C6H12N4 (HMTA)、尿素(CH4N2O)和氢氧化钠(NaOH)。采用ZETA纳米粒度仪、FESEM和EDX研究了不同稳定剂对生长ZnO的粒径、表面形貌和元素组成的影响。观察了浸渍法制备氧化锌溶液的粒径,并记录了HMTA的最小粒径。FESEM图像显示,以HMTA、尿素和NaOH为稳定剂时,ZnO形成了纳米棒、纳米花和颗粒状结构。EDX分析证实了ZnO和TiO2的存在,表明使用稳定剂的样品中锌元素的重量百分比最高。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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