Doğal polimer destekli bir titanyum nanokompozit elektrodun lizin amino aside karşı elektrokimyasal duyarlılığı, seçiciliği ve duyusal özellikleri

Elif Esra Altuner
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Abstract

In this study, chitosan (Chit) supported titanium (Ti) nanoparticles (Ti@Chit NPs) were synthesized by chemical method. Ti@Chit NPs were calculated to be 7.275 ± 2.15 nm and 18.629 nm according to scanning electron microscopy (SEM) and atomic force microscopy (AFM) results, respectively. The synthesized NPs were modified to the electrode and a sensitivity study was carried out against lysine amino acid. It has been determined that the Ti@Chit electrode has a catalytic performance against the amino acid lysine. The limit of detection (LOD) value is estimated to average 0.0041 µM.
本研究采用化学方法合成了壳聚糖(Chit)负载的钛(Ti)纳米粒子(Ti@Chit NPs)。Ti@Chit根据扫描电镜(SEM)和原子力显微镜(AFM)计算NPs分别为7.275±2.15 nm和18.629 nm。将合成的NPs修饰到电极上,并进行了对赖氨酸氨基酸的敏感性研究。已经确定Ti@Chit电极对赖氨酸具有催化性能。检测限(LOD)值估计平均为0.0041µM。
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