Dissipation of dimethoate and fenitrothion in yard long bean (Vigna unguiculata L.) and tomato (Solanum lycopersicum) under supervised field trials

M. Ahmed, M. Prodhan, A. Begum, M. Afroze, N. K. Dutta, D. Sarker
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Abstract

The study was conducted to detect and quantify the residue of dimethoate and fenitrothion in yard long bean and tomato depending on the maximum residue limit (MRL) set by European Union. Four supervised field trials were conducted and sprayed with the recommended dose of dimethoate and fenitrothion at the rate of 2 ml/L of water. Samples were collected at 0, 1, 2, 3, 4, 5, 6, 7, 8, 9, 10 and 11days after spray (DAS). The collected samples were analyzed using Gas Chromatography (GC) coupled with Electron Capture Detector (ECD). The residue of fenitrothion was detected up to 8 DAS in tomato and 9 DAS in yard long bean and the levels of residues were 8.983-0.076 mg/kg in tomato and 6.187- 0.056 mg/kg in yard long bean which were above MRL. No residue was detected at 9 DAS in tomato and 10 DAS in yard long bean. The residue of dimethoate was detected up to 9 DAS in tomato and 10 DAS in yard long bean. The quantities of residues were decrease gradually over time and these were 6.521- 0.034 mg/kg in tomato and 8.590-0.046 mg/kg in yard long bean which were above MRL. No residue was detected at 10 DAS in tomato and 11 DAS in yard long bean. Asian Australas. J. Food Saf. Secur. 2022, 6 (1), 27-34
乐果和杀虫磷在长豇豆和番茄上的耗散试验
根据欧盟规定的最大残留限量(MRL),对长豇豆和番茄中乐果和杀虫硫磷的残留进行了检测和定量研究。进行了四次有监督的田间试验,并以2 ml/L水的速率喷洒推荐剂量的乐果和非硝硫磷。分别于喷雾后0、1、2、3、4、5、6、7、8、9、10、11d采集样品。采用气相色谱(GC)联用电子捕获检测器(ECD)对样品进行分析。在番茄和菜豆中分别检出高达8 DAS和9 DAS的杀虫硫磷残留量,分别为8.983 ~ 0.076 mg/kg和6.187 ~ 0.056 mg/kg,均高于最大残留限量(MRL)。番茄中9个达斯残留量和豇豆中10个达斯残留量均未检出。在番茄中检测到乐果残留量达9 DAS,在豇豆中检测到乐果残留量达10 DAS。随着时间的推移,农药残留量逐渐降低,其中番茄残留量为6.521 ~ 0.034 mg/kg,豇豆残留量为8.590 ~ 0.046 mg/kg,均高于最大残留限量。在番茄中残留10个DAS,在豇豆中残留11个DAS,均未检出残留。亚洲Australas。J.食品安全。安全,2022,6 (1),27-34
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