Synthesis and Study of Structural and Dielectric Properties of Dy-Ho Doped Mn-Zn Ferrite Nanoparticles

K. Manjunatha, V. J. Angadi, B. Fernandes, Keralapura Parthasarathy Ramesh
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引用次数: 4

Abstract

The Dy-Ho doped Mn-Zn Ferrite nanoparticles have been synthesized by solution combustion method using mixture of fuels as glucose and urea. The synthesized samples of structural properties were characterized through XRD (X-ray diffraction) and dielectric properties were studied through impedance analyzer. The XRD patterns of all samples confirms the spinel cubic structure having space group Fd3m. Further all synthesized samples reveal the single-phase formation without any secondary phase. The lattice parameters and hopping lengths were increases with increase of Dy-Ho concentration. SEM micrographs shows the porous nature for all samples. The crystallite size increases with increase of Dy-Ho concentration. The Dielectric properties of all the samples were explained by using Koop’s phenomenological theory. The real part of dielectric constant, imaginary part of dielectric constant and dielectric loss tangent were decreases with increase of frequency. Th AC conductivity increases with increase of frequency. The real part of impedance spectra decreases with increase of frequency for all samples. The Cole-Cole plots shows the one semicircle for all samples. The high ac conductivity and low dielectric loss observed for all samples at high frequency region and this samples are reasonable for power transformer applications at high frequencies.
Dy-Ho掺杂Mn-Zn铁氧体纳米颗粒的合成及结构和介电性能研究
以葡萄糖和尿素为混合燃料,采用溶液燃烧法制备了镝掺杂Mn-Zn铁氧体纳米颗粒。通过XRD (x射线衍射)表征了合成样品的结构性能,并通过阻抗分析仪研究了样品的介电性能。所有样品的XRD谱图均证实尖晶石具有空间群Fd3m的立方结构。此外,所有合成样品均显示单相形成,没有任何二次相。随着Dy-Ho浓度的增加,晶格参数和跳变长度增加。SEM显微图显示了所有样品的多孔性。晶粒尺寸随Dy-Ho浓度的增加而增大。用Koop的现象学理论解释了所有样品的介电性质。介质常数实部、虚部和介质损耗正切随频率的增加而减小。交流电导率随频率的增加而增加。阻抗谱实部随频率的增加而减小。Cole-Cole图显示了所有样本的一个半圆。在高频区域,所有样品的高交流电导率和低介电损耗都是合理的,该样品适用于电力变压器的高频应用。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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