"The influence of graphene oxide on the photocatalytic activity of nanocomposite material"

*А. Zh. Zhumabekov1
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Abstract

"In this paper, is investigated the photocatalytic activity of a nanocomposite material based on titanium and graphene oxides. The sample was obtained by hydrothermal synthesis. The photoactalytic activity of nanocomposites was studied by the transient responce of the photoinduced current. Charge transfer resistances were also investigated using electrochemical impedance spectroscopy. Identification of nanocomposite materials was carried out using Raman and FTIR spectroscopy. This combination shows that there is a connection between the original components. Raman spectroscopy shows that the peaks obtained are characteristic of both titanium dioxide and graphene oxide. At the same time, the ID/IG ratio shows the reduction of graphene oxide during hydrothermal synthesis. And FTIR spectroscopy shows that there is a Ti-O-C bond below the 1000 cm-1 mode. The absorption ability also affects the increase in the photocurrent of the nanocomposite material. Absorption spectra show a shift to the long-wavelength region of light due to the transparency of graphene oxide in the visible region. The concentration of graphene oxide plays an important role in increasing the efficiency of the nanocomposite material. In this work, the concentration of the graphene oxide is equal to 7 wt% with respect to titanium dioxide. Keywords: nanocomposite material, titanium dioxide, graphene oxide, hydrothermal synthesis, photocatalytic activity."
氧化石墨烯对纳米复合材料光催化活性的影响
在本文中,研究了基于钛和石墨烯氧化物的纳米复合材料的光催化活性。样品采用水热法合成。利用光敏电流的瞬态响应研究了纳米复合材料的光催化活性。用电化学阻抗谱法研究了电荷转移电阻。利用拉曼光谱和傅里叶红外光谱对纳米复合材料进行了鉴定。这种组合表明原始组件之间存在联系。拉曼光谱分析表明,所获得的峰具有二氧化钛和氧化石墨烯的特征。同时,在水热合成过程中,氧化石墨烯的ID/IG比值显示出氧化石墨烯的还原。FTIR光谱显示在1000 cm-1模式下存在Ti-O-C键。吸收能力对纳米复合材料光电流的增加也有影响。由于氧化石墨烯在可见光区的透明度,吸收光谱显示出向长波长光区域的偏移。氧化石墨烯的浓度对提高纳米复合材料的效率起着重要的作用。在这项工作中,氧化石墨烯的浓度等于二氧化钛的7 wt%。关键词:纳米复合材料,二氧化钛,氧化石墨烯,水热合成,光催化活性
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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