3D printing of nanocellulose structures infused Epofix resin with improved mechanical properties

M. Latif, Yangxiaozhe Jiang, B. Kumar, Jaehwan Kim
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Abstract

To reduce the dependency on non-renewable resources, high concentration nanocellulose structures are 3D printed, followed by freeze-drying. The freeze-dried structures are impregnated with a commercially available Epofix resin via a widely used vacuum-assisted resin transfer molding process to manufacture nanocellulose-epoxy composites. The porosity, mechanical properties, and thermal stability of the 3D printed structures and composites are investigated by scanning electron microscope (SEM), three-point bending test, and thermal gravimetric analysis (TGA), respectively. The nanocellulose-epoxy composites showed a bending strength and modulus of 30.82 MPa and 2.67 GPa, respectively. The improved mechanical properties of the composites are due to porous free structures after infusion of an Epofix resin, as confirmed by SEM. The thermal stability of the composites increased compared to freeze-dried structures, as confirmed by TGA.
纳米纤维素结构的3D打印注入环氧树脂改善机械性能
为了减少对不可再生资源的依赖,高浓度的纳米纤维素结构被3D打印,然后冷冻干燥。冻干结构通过广泛使用的真空辅助树脂转移成型工艺浸渍商用环氧树脂,以制造纳米纤维素-环氧复合材料。采用扫描电镜(SEM)、三点弯曲试验和热重分析(TGA)分别对3D打印结构和复合材料的孔隙率、力学性能和热稳定性进行了研究。纳米纤维素-环氧复合材料的抗弯强度和模量分别为30.82 MPa和2.67 GPa。扫描电镜证实,复合材料的力学性能的改善是由于注入环氧树脂后的多孔自由结构。热重分析证实,与冻干结构相比,复合材料的热稳定性有所提高。
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