Synthesis and Characterization of Nano Crystalline Mg0.5Zn0.5Fe2O4 Prepared by Co-Precipitation Method

P. Krishna, T. Dayakar, C. P. Vardhini
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Abstract

Mg 0.5 Zn 0.5 Fe 2 O 4 nano crystalline were successfully prepared by employing the co-precipitation method. From XRD it has been fulfilled that single phase spinel structure has been formed at sintering temperature at 900 °C. The particle sizes are in the range of 30 to 40 nm calculated from XRD and SEM graphs. The Mg 0.5 Zn 0.5 Fe 2 O 4 powders prepared at low temperature exhibit good crystal structure, fine grain size and good magnetic properties. The dielectric constant and dielectric loss of sample have shown good frequency stability and low dielectric losses within the measurement range.
共沉淀法制备纳米晶Mg0.5Zn0.5Fe2O4的合成与表征
采用共沉淀法成功制备了mg0.5 zn0.5 fe2o4纳米晶。XRD结果表明,在900℃的烧结温度下形成了单相尖晶石结构。XRD和SEM计算得到的颗粒尺寸在30 ~ 40 nm之间。低温法制备的mg0.5 zn0.5 fe2o4粉体具有良好的晶体结构、晶粒细度和良好的磁性能。样品的介电常数和介电损耗在测量范围内表现出良好的频率稳定性和较低的介电损耗。
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