Electron probe micro analysis and surface resistance measurement investigation of copper chrome coatings on vacuum circuit breaker ceramic surfaces following switching operations

I. Gramberg, M. Kurrat, D. Gentsch
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引用次数: 3

Abstract

Vacuum Interrupters (VIs) are designed for a long operating life. Even after a large number of switching operations they should still provide good arc extinction and be able to withstand high voltages. Switching operations produce substantial masses of metal vapor that condense on the inner component parts of the VI. The Vis are equipped with shields to protect the ceramic surfaces from being coated by metal vapor. Since the first VI was put into service, a large number of shield designs have been developed. If the shield design consists of a floating shield with two end-shields, there are two gaps between these shields. These gaps are necessary for insulation when the VI is in the open position, but during the switching operation metal vapor can flow through these gaps and coat the ceramics. If the deposited area on the alumina ceramics reaches a critical value, the dielectric performance of the VI can become reduced. Standard VIs have been tested with a floating shield and two end shields, that did not overlap the floating shield. The VIs were assembled at the Institute's high power test facility to perform switching operations at different current intensities. After opening the VIs, the coated ceramics were examined. It became clear that, the more switching operations were performed, the darker the deposited layers became. Electron Probe Micro Analysis (EPMA) is a method for surface investigations which was used here to obtain a very detailed view of the thickness of the deposited layers. With EPMA it is possible to detect very thin layers in the range of nanometers. Several coated ceramic surfaces of VIs that had been switched with different current intensities were investigated. In order to provide a better understanding of how strongly different deposited layers can affect the dielectric performance of the VI, surface resistance measurements were carried outdone. These were performed with a high resistance meter, which is able to measure up to 1016Ω using a 1 kV voltage source.
真空断路器陶瓷表面铜铬涂层的电子探针显微分析及表面电阻测量研究
真空断流器(VIs)设计具有较长的工作寿命。即使经过大量的开关操作,它们仍应提供良好的消弧能力,并能够承受高电压。开关操作会产生大量的金属蒸汽,这些金属蒸汽会凝结在VI的内部组件上。Vis配有屏蔽,以保护陶瓷表面不被金属蒸汽覆盖。自第一艘VI投入使用以来,已经开发了大量的屏蔽设计。如果屏蔽设计由带有两个端屏蔽的浮动屏蔽组成,则这些屏蔽之间有两个间隙。当VI处于打开位置时,这些间隙是绝缘所必需的,但在开关操作期间,金属蒸气可以流过这些间隙并涂覆陶瓷。当氧化铝陶瓷上的沉积面积达到临界值时,VI的介电性能会降低。标准VIs已经测试了一个浮动屏蔽和两个端屏蔽,不重叠浮动屏蔽。VIs在研究所的高功率测试设施中组装,以在不同的电流强度下进行开关操作。打开VIs后,对涂层陶瓷进行检测。很明显,进行的开关操作越多,沉积层的颜色就越深。电子探针微观分析(EPMA)是一种表面调查方法,用于获得沉积层厚度的非常详细的视图。使用EPMA可以检测到纳米范围内的非常薄的层。研究了几种不同电流强度开关的VIs涂层陶瓷表面。为了更好地了解不同沉积层对VI介电性能的影响程度,进行了表面电阻测量。这些都是用高阻计进行的,该计能够使用1 kV电压源测量到1016Ω。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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