DETERMINATION OF ENROFLOXACIN RESIDUE IN CHICKEN EGGS USING LIQUID CHROMATOGRAPHY – MASS SPECTROMETRY METHOD

Sadik Heta, F. Shehu, D. Bajraktari
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Abstract

The number of poultry farms in Kosovo is constantly increasing and the need to prevent infectious bacterial infections in poultry has led to the use of antibacterial preparations, which in addition to the beneficial effects of combating these diseases, also poses risk to public health. The purpose of this study was to confirm the presence or absence of enrofloxacin residues in 8 egg samples, after analyzing 180 eggs samples collected at commercial farms in Kosovo with the Elisa Test. The confirmation method used was the Liquid Chromatography Mass Spectrometry. 2 of 8 samples resulted with presence of enrofloxacin residues. The findings suggest that illegal use of enrofloxacine in chicken farms is present and highlight the fact that chicken farmers were using antibiotics as a promoter of egg production and body weight and to reduce the incidence of infectious diseases. Both the tests are performed at the Kosovo Food and Veterinary Laboratory. The testing was performed according to the Commission Decision 2002/657/EC
液相色谱-质谱法测定鸡蛋中恩诺沙星残留
科索沃的家禽养殖场数量不断增加,由于需要防止家禽感染传染性细菌,因此需要使用抗菌制剂,这除了对防治这些疾病有有益作用外,也对公众健康构成威胁。本研究的目的是在对科索沃商业农场收集的180个鸡蛋样本进行Elisa检测后,确认8个鸡蛋样本中是否存在恩诺沙星残留物。采用液相色谱-质谱法对8个样品进行确证,其中2个样品存在恩诺沙星残留。研究结果表明,养鸡场存在非法使用恩诺沙辛的情况,并强调养鸡场使用抗生素是为了促进产蛋量和体重,并减少传染病的发病率。这两项检测都在科索沃食品和兽医实验室进行。测试是根据委员会决定2002/657/EC进行的
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