Oxygen detection using nanoporous anodized aluminum oxide sensors

S. Vunnam, Alekha Andolu, M. Kocanda, M. Haji-Sheikh, D. Ballantine, A. Bose
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Abstract

The objective of this work has been the analysis of the impedance variation of nanostructured sensors in the presence of several gases at different temperatures. This sensor employs platinum nanowires grown in anodic aluminum oxide to detect the gases. Silicon wafers were oxidized to form silicon dioxide and were sputter deposited with titanium tungstide and aluminum metal. The aluminum film was subsequently anodized to form nonporous anodic aluminum oxide. Platinum metal was filled in these pores by the process of electropolymerization to form encapsulated nanowires. Surface morphology characteristics were determined using atomic force microscopy and scanning electron microscopy. A subsequent metallization process using evaporation deposited gold metal to form electrical contacts. Variations in the electrical response of the sensor in the presence of hydrogen, nitrogen and oxygen at 5°C, 25°C and 40°C are presented in this work.
利用纳米多孔阳极氧化铝传感器进行氧检测
这项工作的目的是分析纳米结构传感器在不同温度下几种气体存在时的阻抗变化。这种传感器采用生长在阳极氧化铝中的铂纳米线来检测气体。将硅片氧化生成二氧化硅,并与钨化钛和铝金属进行溅射沉积。随后对铝膜进行阳极氧化,形成无孔阳极氧化铝。通过电聚合的方法将铂金属填充在这些孔中,形成包封的纳米线。用原子力显微镜和扫描电镜测定了表面形貌特征。随后的金属化过程使用蒸发沉积金金属形成电触点。在5°C、25°C和40°C下,传感器在氢、氮和氧存在下的电响应变化。
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