{"title":"Utilization of Coconut Waste as a Basic Material for Making Carbon Dots with Acid Oxidation Method","authors":".. Marpongahtun, .. Irmayani, S. A.","doi":"10.5220/0010139700002775","DOIUrl":null,"url":null,"abstract":": Utilization of coconut shell soot as raw material for making carbon dots has been successfully carried out. This study used coconut shell soot with 5 M HNO 3 acid oxidation method which is then the Carbon dots characteristics were determined using UV light, UV-Vis, TEM analysis, and functional group analysis with FT-IR. Coconut shell soot is obtained by pyrolysis method. The heating process using a furnace carried out for 2 hours at 400 °C. Carbon dots produced by heating with 5 M HNO 3 for 12 hours at 100 °C, centrifuged and dialysis. The yield of carbon dots was 87%. The FT-IR spectrum shows that the Carbon dots formed produce OH group absorption at 3396 cm -1 , absorption of C = C at wave number 1637 cm -1 , absorption of CO groups, and CH at wave number 1339 cm -1 , and 835 cm -1 . Analysis with Transmission Electron Microscopy shows that carbon dots has an average diameter of 1.50 nm. Absorbance spectrum analysis (UV-Vis) results in the appearance of new uptake showing the electron transition at a wavelength of 307 nm and giving green fluorescence under UV light.","PeriodicalId":257157,"journal":{"name":"Proceedings of the 1st International MIPAnet Conference on Science and Mathematics","volume":"27 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Proceedings of the 1st International MIPAnet Conference on Science and Mathematics","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.5220/0010139700002775","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
Abstract
: Utilization of coconut shell soot as raw material for making carbon dots has been successfully carried out. This study used coconut shell soot with 5 M HNO 3 acid oxidation method which is then the Carbon dots characteristics were determined using UV light, UV-Vis, TEM analysis, and functional group analysis with FT-IR. Coconut shell soot is obtained by pyrolysis method. The heating process using a furnace carried out for 2 hours at 400 °C. Carbon dots produced by heating with 5 M HNO 3 for 12 hours at 100 °C, centrifuged and dialysis. The yield of carbon dots was 87%. The FT-IR spectrum shows that the Carbon dots formed produce OH group absorption at 3396 cm -1 , absorption of C = C at wave number 1637 cm -1 , absorption of CO groups, and CH at wave number 1339 cm -1 , and 835 cm -1 . Analysis with Transmission Electron Microscopy shows that carbon dots has an average diameter of 1.50 nm. Absorbance spectrum analysis (UV-Vis) results in the appearance of new uptake showing the electron transition at a wavelength of 307 nm and giving green fluorescence under UV light.
利用椰壳烟灰为原料制备碳点已成功。本研究采用5 M hno3酸氧化法对椰壳烟灰进行了碳点特性的测定,采用紫外光、紫外可见光谱、透射电镜和红外光谱对其进行了官能团分析。采用热解法制备椰壳烟尘。加热过程采用加热炉在400°C下进行2小时。用5 M hno3在100℃下加热12小时,离心和透析产生的碳点。碳点的收率为87%。FT-IR光谱表明,形成的碳点在3396 cm -1处产生OH基团吸收,在1637 cm -1处产生C = C吸收,在1339 cm -1和835 cm -1处产生CO基团吸收和CH吸收。透射电镜分析表明,碳点的平均直径为1.50 nm。吸收光谱分析(UV- vis)结果显示在307 nm波长处出现新的吸收,并在紫外光下发出绿色荧光。