Utilization of Coconut Waste as a Basic Material for Making Carbon Dots with Acid Oxidation Method

.. Marpongahtun, .. Irmayani, S. A.
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Abstract

: Utilization of coconut shell soot as raw material for making carbon dots has been successfully carried out. This study used coconut shell soot with 5 M HNO 3 acid oxidation method which is then the Carbon dots characteristics were determined using UV light, UV-Vis, TEM analysis, and functional group analysis with FT-IR. Coconut shell soot is obtained by pyrolysis method. The heating process using a furnace carried out for 2 hours at 400 °C. Carbon dots produced by heating with 5 M HNO 3 for 12 hours at 100 °C, centrifuged and dialysis. The yield of carbon dots was 87%. The FT-IR spectrum shows that the Carbon dots formed produce OH group absorption at 3396 cm -1 , absorption of C = C at wave number 1637 cm -1 , absorption of CO groups, and CH at wave number 1339 cm -1 , and 835 cm -1 . Analysis with Transmission Electron Microscopy shows that carbon dots has an average diameter of 1.50 nm. Absorbance spectrum analysis (UV-Vis) results in the appearance of new uptake showing the electron transition at a wavelength of 307 nm and giving green fluorescence under UV light.
利用椰子废料作为酸氧化法制备碳点的基础材料
利用椰壳烟灰为原料制备碳点已成功。本研究采用5 M hno3酸氧化法对椰壳烟灰进行了碳点特性的测定,采用紫外光、紫外可见光谱、透射电镜和红外光谱对其进行了官能团分析。采用热解法制备椰壳烟尘。加热过程采用加热炉在400°C下进行2小时。用5 M hno3在100℃下加热12小时,离心和透析产生的碳点。碳点的收率为87%。FT-IR光谱表明,形成的碳点在3396 cm -1处产生OH基团吸收,在1637 cm -1处产生C = C吸收,在1339 cm -1和835 cm -1处产生CO基团吸收和CH吸收。透射电镜分析表明,碳点的平均直径为1.50 nm。吸收光谱分析(UV- vis)结果显示在307 nm波长处出现新的吸收,并在紫外光下发出绿色荧光。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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