Structural and magnetic properties of Tb0.27Dy0.73Fe2-xNbx (x = 0, 0.05, 0.1 and 0.2)

Hari Babu, A. Subrahmanyam, M. Palit, S. Pandian
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Abstract

In this paper, the effect of substituting Fe partially by the 4d element Nb on the structural and magnetic properties of Tb0.27Dy0.73Fe2 is reported. Polycrystalline compounds of Tb0.27Dy0.73Fe2-xNbx (x = 0, 0.05, 0.1 and 0.2) were prepared by arc melting the constituent elements (rare earths-99.9 % pure, Fe and Nb -99.95 % pure) in an arc furnace under argon atmosphere. The ingots were annealed in vacuum at 950degC for a week. X-ray diffraction patterns of these compounds were taken using a PANalytical X-ray diffractrometer. Magnetization up to 12 kOe and Curie temperature (Tc) measurements were carried out using a PAR-155 vibrating sample magnetometer (VSM). Magnetostriction measurements at room temperature were carried out employing strain gauge method.
Tb0.27Dy0.73Fe2-xNbx (x = 0、0.05、0.1和0.2)的结构和磁性能
本文报道了用4d元素Nb部分取代Fe对Tb0.27Dy0.73Fe2结构和磁性能的影响。在氩气氛下,用电弧炉熔炼稀土纯度为99.9%,Fe和Nb纯度为99.95%的元素,制备了Tb0.27Dy0.73Fe2-xNbx (x = 0、0.05、0.1和0.2)多晶化合物。钢锭在950摄氏度的真空中退火一周。这些化合物的x射线衍射图是用PANalytical x射线衍射仪拍摄的。使用PAR-155振动样品磁强计(VSM)测量了高达12 kOe的磁化强度和居里温度(Tc)。采用应变片法进行了室温下的磁致伸缩测量。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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