Synthesis, Characterization and Dielectric properties of Nanoparticles of Cobalt Doped Ferrite (Cox Fe1-x Fe2 O4)

Priyanka Gupta, Dr. Ravi Kumar Vijai
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Abstract

Ferrites, a recently uncovered category of materials, have found extensive application in various critical domains. Among them, cobalt ferrites stand out as hard magnetic materials with exceptional coercivity.. We successfully prepared cobalt ferrites by using nanocrystalline powers by Sol gel method. In our study Crystalline, Magnetic nanoparticles of Cobalt ferrites (Cox Fe1-x Fe2 O4) (x = 0.4, 0.5, 0.6, 0.8) were synthesized by Sol Gel Method using ferric chloride and cobalt nitrate with NaOH as a reactant. Structural characteristics of samples were determined by X-Ray diffraction and TEM. Particle size found between 8.8 nm to 14.26 nm using Debye Scherrer method. Lattice constant decreases as the value of ‘x’ increases. Dielectric properties were investigated using impedance analyser. The relative dielectric constant and loss tangents of ferrites a function of frequency (1kHz-30MHz) was investigated at room temperature, both parameter decreases as frequency increases.
纳米钴掺杂铁氧体(Cox Fe1-x Fe2 O4)的合成、表征及介电性能
铁氧体是近年来发现的一类材料,在各种关键领域得到了广泛的应用。其中,钴铁氧体作为具有特殊矫顽力的硬磁性材料脱颖而出。采用溶胶-凝胶法制备了钴铁氧体。本文以氯化铁和硝酸钴为原料,以NaOH为反应物,采用溶胶-凝胶法制备了晶体磁性钴铁氧体纳米粒子(Cox Fe1-x Fe2 O4) (x = 0.4, 0.5, 0.6, 0.8)。采用x射线衍射和透射电镜对样品进行了结构表征。使用Debye Scherrer方法发现粒径在8.8 nm至14.26 nm之间。晶格常数随着x值的增大而减小。用阻抗分析仪对其介电性能进行了研究。研究了室温下铁氧体的相对介电常数和损耗切线随频率(1khz ~ 30mhz)的变化规律,两者随频率的增加而减小。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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