Microplastic Analysis at Sea Water and Sediment in the Mahitam Island Lampung Bay using FT-IR

Nita Sari, E. Widiastuti, G. Pratami, T. Tugiyono
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Abstract

The amount of garbage that accumulates in the waters causes environmental damage which is getting worse. The breakdown of plastic waste into smaller particles that have been degraded is called microplastic. This study aims to analyze the number of particles, shapes, and types of microplastic polymers found in the water and sediments of Mahitam Island. The research location was determined by purposive random sampling with three stations based on plastic sources, namely Station I, Station II, and Station III, which had different characteristics from laboratory-based testing for seawater and sediment. Microplastic analysis on seawater samples was carried out by adding a solution of 70% ethanol, 30% H2O2, and 30% NaCl, and on sediment samples was carried out by adding a solution of FeSO4 (0.05 M), NaCl, and 30% H2O2. The content of the number of particles and the shape of microplastics were analyzed using a microscope, while the analysis of microplastic polymers using FT-IR. The first thing to do is to extract microplastics The forms of microplastic found are Fiber, Film, Fragments, and Pellets. The highest number of microplastic particles was the type of film for water samples at Station 1 and Station 2 for sediment samples. The types of polymers found in water and sediments on Mahitam Island are polyvinyl chloride (PVC), polyethylene (PE), polypropylene (PP), and polystyrene (PS) which come from plastic waste. Microplastics are known to originate from the use of plastic originating from tourist activities and originating from the sea currents of Mahitam Island.
利用傅里叶变换红外光谱分析马淡岛楠榜湾海水和沉积物的微塑料
堆积在水中的垃圾数量对环境造成了越来越严重的破坏。塑料垃圾分解成更小的被降解的颗粒被称为微塑料。这项研究旨在分析在Mahitam岛的水和沉积物中发现的微塑料聚合物的颗粒数量、形状和类型。研究地点采用有目的随机抽样的方法确定,基于塑料源的3个站点分别为1、2、3个站点,这些站点与基于实验室的海水和沉积物检测具有不同的特点。海水样品加入70%乙醇、30% H2O2和30% NaCl溶液进行微塑性分析,沉积物样品加入0.05 M FeSO4、NaCl和30% H2O2溶液进行微塑性分析。用显微镜分析了微塑料的颗粒数量和形状,用红外光谱分析了微塑料聚合物。首先要做的是提取微塑料,发现的微塑料的形式有纤维、薄膜、碎片和颗粒。1号站的水样和2号站的沉积物样品的薄膜类型的微塑料颗粒数量最多。在Mahitam岛的水和沉积物中发现的聚合物类型是聚氯乙烯(PVC),聚乙烯(PE),聚丙烯(PP)和聚苯乙烯(PS),它们来自塑料废物。众所周知,微塑料源于旅游活动中塑料的使用和Mahitam岛的海流。
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