STRUCTURAL AND MAGNETO CONDUCTIVITY STUDIES OF NIO/SMBA2CU3O7-Δ SUPERCONDUCTING COMPOSITE

H. Basma, S. Rmeid, R. Awad, M. Said
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Abstract

In this work, we investigate the effect of NiO nanoparticles' addition on the structure, superconductivity, and magneto conductivity for the SmBa2Cu3O7-δ phase. Composite nano/superconductor of (NiO)x/SmBa2Cu3O7-δ (0.00≤x≤0.12 wt.%) were prepared by conventional solid-state reaction technique and characterized by X-ray powder diffraction (XRD) and scanning electron microscopy (SEM). The orthorhombic structure was maintained whereas the lattice parameters showed unsystematic variations with the NiO nanoparticles addition. The superconducting transition temperature Tc, determined from electrical resistivity measurements, showed an enhancement with x up to 0.04wt.% followed by a reduction with higher NiO additions. The Aslamazov–Larkin (AL) model was employed to analyze the magneto conductivity. The model allowed to determine the coherence lengths along c-axis ξc(0) and along ab plane ξab(0). Moreover, the anisotropy parameter Г increase with the increase of NiO nanoparticles addition.
nio / smba2cu3o7 -Δ超导复合材料的结构和导电性研究
在这项工作中,我们研究了NiO纳米颗粒的加入对SmBa2Cu3O7-δ相的结构、超导性和导电性的影响。采用常规固相反应法制备了(NiO)x/SmBa2Cu3O7-δ(0.00≤x≤0.12 wt.%)复合纳米超导体,并用x射线粉末衍射(XRD)和扫描电镜(SEM)对其进行了表征。随着NiO纳米颗粒的加入,晶格参数呈现出非系统的变化。超导转变温度Tc,由电阻率测量确定,显示出x增加到0.04wt。%,然后加入更多的NiO。采用Aslamazov-Larkin (AL)模型分析其磁导率。该模型可以确定沿c轴ξc(0)和沿ab平面ξab(0)的相干长度。各向异性参数Г随NiO纳米颗粒添加量的增加而增大。
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