Quantitation of benzoic and sorbic acid levels from green olives by high-performance liquid chromatography

A. A. Bayizit, T. Ozcan, L. Y. Ersan, Nihal Barlak, Gokce Hoca
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Abstract

Olive fruit is utilized in two forms: table olives and oil. In our country, food additives that are added consciously and deliberately are used in table olive production to bring the appearance and flavour of olives to the state desired by the consumer, to prevent the deterioration of olives and to extend their shelf life. In Turkey, the amount of preservatives to be added to foods should be compatible with the Turkish Food Codex. This study was carried out to determine the amounts of benzoic ands orbic acids added to extend the shelf life in pickled green olives provided from Bursa market using the HPLC method and to find out whether the findings obtained are within the legal limits envisaged in the Regulation on Food Additives. Among 100 green olive samples supplied, while sorbic acid and benzoic acid were not detected in 79 green olive samples. Sorbic acid was observed in 10 of the samples and benzoic acid was in 1 of the samples, however both acids were detected in 11 of the samples. The detected amounts of sorbic acid ranged between 49,103 and 204,989mg kg-1, while benzoic acid values were within 142,352-153,453 mg kg-1. The preservatives were not detected in the 4 green olive samples which were above 7% of the salt content, whilst they were observed in 20 of the samples with salt ratio below 7%. However their detected amounts were within the levels allowed by Turkish Food Codex.
高效液相色谱法测定绿橄榄中苯甲酸和山梨酸含量
橄榄果有两种用途:食用橄榄和橄榄油。在我国,食用橄榄生产中使用有意识、刻意添加的食品添加剂,使橄榄的外观和风味达到消费者所希望的状态,防止橄榄变质,延长其保质期。在土耳其,添加到食品中的防腐剂的数量应符合土耳其食品法典的规定。本研究旨在利用高效液相色谱法确定为延长布尔萨市场提供的腌绿橄榄的保质期而添加苯甲酸和硼酸的量,并确定所获得的结果是否在《食品添加剂规例》所规定的法定限度内。在所提供的100份绿橄榄样品中,79份绿橄榄样品未检出山梨酸和苯甲酸。10份样品中检出山梨酸,1份样品中检出苯甲酸,11份样品中检出两种酸。山梨酸的检测量在49,103至204,989mg kg-1之间,苯甲酸的检测值在142,352至153,453 mg kg-1之间。在含盐量高于7%的4个绿橄榄样品中未检测到防腐剂,而在含盐量低于7%的20个样品中发现了防腐剂。然而,检测到的含量在土耳其食品法典允许的水平范围内。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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