Optimization strategies and artifacts of time-involved small-angle neutron scattering experiments.

IF 6.1 3区 材料科学 Q1 Biochemistry, Genetics and Molecular Biology
Denis Mettus, Alfonso Chacon, Andreas Bauer, Sebastian Mühlbauer, Christian Pfleiderer
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引用次数: 0

Abstract

Kinetic small-angle neutron scattering provides access to the microscopic properties of mesoscale systems under slow, periodic perturbations. By interlocking the phases of neutron pulse, sample modulation and detector signal, time-involved small-angle neutron scattering experiments (TISANE) allow one to exploit the neutron velocity spread and record data without major sacrifice in intensity at timescales down to microseconds. This article reviews the optimization strategies of TISANE that arise from specific aspects of the process of data acquisition and data analysis starting from the basic principles of operation. Typical artifacts of data recorded in TISANE due to the choice of time binning and neutron chopper pulse width are illustrated by virtue of the response of the skyrmion lattice in MnSi under periodic changes of the direction of the stabilizing magnetic field.

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含时小角中子散射实验的优化策略与伪影。
动力学小角中子散射提供了在缓慢、周期性扰动下中尺度系统微观特性的途径。通过联锁中子脉冲、样品调制和探测器信号的相位,时间相关的小角度中子散射实验(TISANE)允许人们利用中子速度传播和记录数据,而不会在时间尺度低至微秒的强度上做出重大牺牲。本文从操作的基本原理出发,从数据采集和数据分析过程的具体方面综述了TISANE的优化策略。利用稳定磁场方向周期性变化下MnSi中skyrmion晶格的响应,说明了TISANE中记录数据的典型伪影是由于时间束和中子斩波脉冲宽度的选择造成的。
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来源期刊
CiteScore
10.00
自引率
3.30%
发文量
178
审稿时长
4.7 months
期刊介绍: Many research topics in condensed matter research, materials science and the life sciences make use of crystallographic methods to study crystalline and non-crystalline matter with neutrons, X-rays and electrons. Articles published in the Journal of Applied Crystallography focus on these methods and their use in identifying structural and diffusion-controlled phase transformations, structure-property relationships, structural changes of defects, interfaces and surfaces, etc. Developments of instrumentation and crystallographic apparatus, theory and interpretation, numerical analysis and other related subjects are also covered. The journal is the primary place where crystallographic computer program information is published.
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