铜与3,5-吡啶二羧酸和IMZ配合物的合成、晶体结构和性能

Yanfeng Huang, Zhan-wang Shi, Qiaoli Qin, Xuewu Huang, Jian-gang Chen, S.-J. Cao, L. Qin, X. Yin
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引用次数: 1

摘要

六坐标3,5-吡啶二羧酸和咪唑与氯化铜在乙醇水溶液、水溶液和氯化铜在N,N-二甲基甲酰胺水溶液中反应生成配合物Cu(IMZ)(3,5-pdc)4] (IMZ:咪唑)。通过元素分析、红外光谱、x射线晶体衍射、循环伏安法和热重法对配合物进行了表征。铜原子由3,5-吡啶二羧酸和咪唑配体桥接成二维结构。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis, Crystal Structure, and Properties of a Cu Complex With 3,5-Pyridinedicarboxylic Acid and IMZ
A hexa-coordinate 3,5-pyridinedicarboxylic acid and imidazole react with copper chloride in the ethanol aqueous solution, water solution, and copper chloride in an N,N-dimethylformamide aqueous to give the complex Cu(IMZ)(3,5-pdc)4] (IMZ: imidazole). The complex has been characterized by elemental analysis, IR spectra, X-ray crystal diffraction, cyclic voltammetry, and thermogravimetry. The Cu atom is bridged by 3,5-pyridinedicarboxylic acid and imidazole ligand into 2D structure.
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