{"title":"特异性3A, 3C, 3e -0-三磺化β-环糊精","authors":"K. Fujita, T. Tahara, H. Yamamura, T. Koga","doi":"10.5458/JAG1972.38.205","DOIUrl":null,"url":null,"abstract":"3A, 3C, 3E-O-tris(β-naphthylsulfonyl)-β-cyclodextrin was selectively prepared by the reaction of β-cyclodextrin with β-naphthylsulfonyl chloride in an alkaline solution. The structure determination was carried out by use of a regiochemical relationship between a 3-O-sulfonylcyclodextrin with a 6-O-sulfonylcyclodextrin through a 3, 6-anhydrocyclodextrin.","PeriodicalId":17372,"journal":{"name":"Journal of the Japanese Society of Starch Science","volume":"136 1","pages":"205-209"},"PeriodicalIF":0.0000,"publicationDate":"1991-06-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Specific 3A, 3C, 3E-0-Trisulfonylation of β-cyclodextrin\",\"authors\":\"K. Fujita, T. Tahara, H. Yamamura, T. Koga\",\"doi\":\"10.5458/JAG1972.38.205\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"3A, 3C, 3E-O-tris(β-naphthylsulfonyl)-β-cyclodextrin was selectively prepared by the reaction of β-cyclodextrin with β-naphthylsulfonyl chloride in an alkaline solution. The structure determination was carried out by use of a regiochemical relationship between a 3-O-sulfonylcyclodextrin with a 6-O-sulfonylcyclodextrin through a 3, 6-anhydrocyclodextrin.\",\"PeriodicalId\":17372,\"journal\":{\"name\":\"Journal of the Japanese Society of Starch Science\",\"volume\":\"136 1\",\"pages\":\"205-209\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"1991-06-30\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of the Japanese Society of Starch Science\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.5458/JAG1972.38.205\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of the Japanese Society of Starch Science","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.5458/JAG1972.38.205","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
摘要
通过β-环糊精与β-萘磺酰氯在碱性溶液中选择性反应，制备了3A, 3C, 3e - o -三(β-萘磺酰)-β-环糊精。利用3- o -磺酰基环糊精与6- o -磺酰基环糊精通过3,6 -无氢环糊精之间的区域化学关系对其结构进行了测定。
Specific 3A, 3C, 3E-0-Trisulfonylation of β-cyclodextrin
3A, 3C, 3E-O-tris(β-naphthylsulfonyl)-β-cyclodextrin was selectively prepared by the reaction of β-cyclodextrin with β-naphthylsulfonyl chloride in an alkaline solution. The structure determination was carried out by use of a regiochemical relationship between a 3-O-sulfonylcyclodextrin with a 6-O-sulfonylcyclodextrin through a 3, 6-anhydrocyclodextrin.
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