一种新的测定软饮料中苯甲酸钠的有效光谱方法

Manda Pravalika, Jorige Archana
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引用次数: 3

摘要

食品分析最令人信服的原因之一是确保它对消费者和生产者都是安全的。苯甲酸钠是一种流行的食品成分,可以在各种食品和饮料中找到。根据国际协调会议(ICH Q2 R1)的原理,建立了一种快速简便的紫外区苯甲酸钠测定方法。用蒸馏水配制标准液和样品溶液。在224nm处获得最大吸光度(λmax)。在1 ~ 40µg/ml范围内,标定曲线呈线性。日内和日间的rsd分别为0.08和0.17。LOD和LOQ分别为0.031和0.093。稳健性的% RSD为0.86,而坚固性的% RSD为0.35。该方法快速、简便、准确、经济,适用于苯甲酸钠饮料的常规质量控制。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
A New Validated Spectroscopic Method for the estimation of Sodium Benzoate in Soft drinks
One of the most compelling reasons for food analysis is to ensure that it is safe for both consumers and producers. Sodium benzoate is a popular food ingredient that can be found in a variety of foods and beverages. To measure sodium benzoate in the UV-region, a rapid and simple Spectrophotometric method was devised and validated according to International Conference on Harmonization (ICH Q2 R1) principles. Distilled water was used to make the standard and sample solutions. At 224nm, the maximum absorbance (λmax) was obtained. In the range of 1-40 µg/ml, the calibration curve was linear. The intra-day and inter-day percent RSDs were found to be 0.08 and 0.17, respectively. 0.031 and 0.093 were found to be the LOD and LOQ, respectively. The % RSD for robustness was found to be 0.86, while the % RSD for ruggedness was found to be 0.35. The proposed method was rapid, simple, precise and economic and can be adapted to routine quality control of beverages having Sodium benzoate.
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