综述:不同基质的全汽化固相微萃取方法

Yunes M. M. A. Alsayadi, Saahil Arora
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引用次数: 2

摘要

全汽化固相微萃取(TV-SPME)是一种用特定溶剂溶解分析物的萃取技术。然后将少量的溶剂放入SPME瓶中。然后,溶剂在SPME瓶中汽化,对SPME纤维的顶空进行取样。因此,分析物在顶空和液体样品之间的分划相被省略了。平衡相仍然是分析物在顶空和SPME之间的分配。goodpaste于2014年推出了TV-SPME,与液体注入方法相比,它可以提高采收率。本文讨论了TV-SPME的不同方面,包括其对抽样技术、理论部分、抽样程序和方法优化的影响。对其应用给予了特别注意。在相关数据库中进行了全面的文献研究,总结了对该技术所做的研究工作。在TV-SPME中,液体样品完全汽化,基质效应较小,吸附效果较好。该方法无需制样,耗材少,可自动完成。此外,TV-SPME能够经济高效地提取不同的基质。本文综述了TV-SPME的相关方面。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
A review: Total vaporization solid-phase microextraction procedure in different matrixes
Total vaporization solid-phase microextraction (TV-SPME) is a type of extraction technique in which a specific solvent dissolves the analyte. Then a tiny amount of solvent is taken to the vial of SPME. Then, the solvent vaporizes in the SPME vial, and sampling is carried out on the headspace of the SPME fiber. As a result, the partitioning phase of the analyte between the headspace and liquid sample is omitted. The equilibrium phase remains the analyte partitioning between the headspace and SPME. TV-SPME was introduced in 2014 by Goodpaster to increase the recovery compared to the liquid injection method. This review discusses different aspects of TV-SPME, including its impact on sampling techniques, theoretical part, sampling procedure, and method optimization. Special attention was paid to its applications. A comprehensive literature study was conducted in the relevant databases to summarize the research work that has been done on this technique. In TV-SPME, the liquid samples completely vaporized and had a less matrix effect and better adsorption. This method needs no sample preparation, consumes less supply, and can be done automatically. Also, TV-SPME enables a cost-effective and efficient extraction for different matrixes. This review summarizes aspects related to TV-SPME.
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