Liangwen Liu, Xin Wu, Jingyi Wang, N. Tang, Shuang Li, Xianjv Zhang, Mei Yang
{"title":"Ca和P改性钛合金微弧氧化涂层羟基磷灰石的形成","authors":"Liangwen Liu, Xin Wu, Jingyi Wang, N. Tang, Shuang Li, Xianjv Zhang, Mei Yang","doi":"10.1080/00202967.2022.2087944","DOIUrl":null,"url":null,"abstract":"ABSTRACT A Simulated Body Fluid (SBF) treatment was performed to modify the surface of a TiO2-based coating containing Ca and P prepared by micro-arc oxidation (MAO). Scanning electron microscopy (SEM), X-ray diffraction (XRD), and X-Ray Photoelectron Spectroscopy (XPS) were employed to characterise the composition and morphology of the immersed Ca-P containing coating. The coating primarily presents a porous structure, which is mainly composed of anatase, rutile, CaP, and Nb2O5.The biological activity of the coating was determined by immersing in SBF for 5 days, showing hydroxyapatite (HA) formed on the surface of the coating and also revealing the good corrosion resistance of the coating in SBF. Finally, a lower MAO coating contact angle with SBF solution than that of TLM Ti alloy was obtained in the compatibility test, indicating that the coating has good compatibility with SBF.","PeriodicalId":23251,"journal":{"name":"Transactions of the IMF","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2022-07-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"Hydroxyapatite formation of Ca and P modified micro-arc oxidation coating on Ti alloy\",\"authors\":\"Liangwen Liu, Xin Wu, Jingyi Wang, N. Tang, Shuang Li, Xianjv Zhang, Mei Yang\",\"doi\":\"10.1080/00202967.2022.2087944\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"ABSTRACT A Simulated Body Fluid (SBF) treatment was performed to modify the surface of a TiO2-based coating containing Ca and P prepared by micro-arc oxidation (MAO). Scanning electron microscopy (SEM), X-ray diffraction (XRD), and X-Ray Photoelectron Spectroscopy (XPS) were employed to characterise the composition and morphology of the immersed Ca-P containing coating. The coating primarily presents a porous structure, which is mainly composed of anatase, rutile, CaP, and Nb2O5.The biological activity of the coating was determined by immersing in SBF for 5 days, showing hydroxyapatite (HA) formed on the surface of the coating and also revealing the good corrosion resistance of the coating in SBF. Finally, a lower MAO coating contact angle with SBF solution than that of TLM Ti alloy was obtained in the compatibility test, indicating that the coating has good compatibility with SBF.\",\"PeriodicalId\":23251,\"journal\":{\"name\":\"Transactions of the IMF\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2022-07-08\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Transactions of the IMF\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1080/00202967.2022.2087944\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Transactions of the IMF","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1080/00202967.2022.2087944","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Hydroxyapatite formation of Ca and P modified micro-arc oxidation coating on Ti alloy
ABSTRACT A Simulated Body Fluid (SBF) treatment was performed to modify the surface of a TiO2-based coating containing Ca and P prepared by micro-arc oxidation (MAO). Scanning electron microscopy (SEM), X-ray diffraction (XRD), and X-Ray Photoelectron Spectroscopy (XPS) were employed to characterise the composition and morphology of the immersed Ca-P containing coating. The coating primarily presents a porous structure, which is mainly composed of anatase, rutile, CaP, and Nb2O5.The biological activity of the coating was determined by immersing in SBF for 5 days, showing hydroxyapatite (HA) formed on the surface of the coating and also revealing the good corrosion resistance of the coating in SBF. Finally, a lower MAO coating contact angle with SBF solution than that of TLM Ti alloy was obtained in the compatibility test, indicating that the coating has good compatibility with SBF.
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