{"title":"新型氨基酸基偶氮染料镨(III)配合物的合成及光谱表征","authors":"Man Singh, Sushma Anant","doi":"10.1155/2012/767080","DOIUrl":null,"url":null,"abstract":"A new Praseodymium (Pr) (III) complex has been synthesized and characterized by using a new amino acid-based (leucine) azo dye such as N,N-dimethylazoleucine (L1) and 1,10 phenanthroline (L2). Reaction of Pr(III) ion with L1 and L2 in 1 : 2 : 1 ratio in alcoholic medium has been carried out with general formula [Pr(L1)2(L2)(H2O)2]. Elemental analysis, comparative FT-IR, and 1HNMR spectral studies of Pr(III) complex with ligands have been shown in this paper.","PeriodicalId":14074,"journal":{"name":"International Journal of Inorganic Chemistry","volume":"148 1","pages":"1-6"},"PeriodicalIF":0.0000,"publicationDate":"2012-02-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"5","resultStr":"{\"title\":\"Synthesis and Spectral Characterization of Praseodymium(III) Complex with New Amino Acid-Based Azo Dye\",\"authors\":\"Man Singh, Sushma Anant\",\"doi\":\"10.1155/2012/767080\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"A new Praseodymium (Pr) (III) complex has been synthesized and characterized by using a new amino acid-based (leucine) azo dye such as N,N-dimethylazoleucine (L1) and 1,10 phenanthroline (L2). Reaction of Pr(III) ion with L1 and L2 in 1 : 2 : 1 ratio in alcoholic medium has been carried out with general formula [Pr(L1)2(L2)(H2O)2]. Elemental analysis, comparative FT-IR, and 1HNMR spectral studies of Pr(III) complex with ligands have been shown in this paper.\",\"PeriodicalId\":14074,\"journal\":{\"name\":\"International Journal of Inorganic Chemistry\",\"volume\":\"148 1\",\"pages\":\"1-6\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2012-02-29\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"5\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"International Journal of Inorganic Chemistry\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1155/2012/767080\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Journal of Inorganic Chemistry","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1155/2012/767080","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Synthesis and Spectral Characterization of Praseodymium(III) Complex with New Amino Acid-Based Azo Dye
A new Praseodymium (Pr) (III) complex has been synthesized and characterized by using a new amino acid-based (leucine) azo dye such as N,N-dimethylazoleucine (L1) and 1,10 phenanthroline (L2). Reaction of Pr(III) ion with L1 and L2 in 1 : 2 : 1 ratio in alcoholic medium has been carried out with general formula [Pr(L1)2(L2)(H2O)2]. Elemental analysis, comparative FT-IR, and 1HNMR spectral studies of Pr(III) complex with ligands have been shown in this paper.