ATO中Sb3+/Sb5+含量比的快速估算方法

Q2 Chemistry

Zeitschrift Fur Kristallographie Pub Date : 2007-01-01 DOI:10.1524/ZKRI.2007.2007.SUPPL_26.67

B. Gržeta, E. Tkalčec, C. Goebbert, M. Takeda, Masashi Takahashi

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引用次数: 0

摘要

介绍了一种估算掺锑氧化锡(ATO)中Sb^(3+)/Sb^(5+)含量比的方法。它包括ATO样品在狭窄的2 θ范围内的XRD谱图的测量和衍射线110和101的单独剖面拟合。谱线110和101的半最大值全宽比(FWHM) FWHM_(110)/FWHM_(101)与ATO样品中Sb^(3+)/Sb^(5+)含量比呈线性相关。该方法是通过对ATO样品的XRD和^(121)sb -穆斯堡尔光谱研究得出的。

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Method for quick estimation of the Sb3+/Sb5+content ratio in ATO

A method for estimation of the Sb^(3+)/Sb^(5+) content ratio in antimony-doped tin oxide (ATO) is described. It involves measuring of XRD pattern of ATO sample in a narrow 2theta range and individual profile fitting of diffraction lines 110 and 101. The ratios of full-widths at half-maximum (FWHM) of the lines 110 and 101, FWHM_(110)/FWHM_(101), is linearly correlated with the Sb^(3+)/Sb^(5+) content ratio in the ATO sample. The method resulted from the XRD and ^(121)Sb-Mossbauer spectroscopy investigation of ATO samples.

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来源期刊

Zeitschrift Fur Kristallographie 物理-晶体学

CiteScore

1.47

自引率

0.00%

发文量

审稿时长

3 months

期刊介绍： Zeitschrift für Kristallographie International journal for structural, physical, and chemical aspects of crystalline materials ISSN 0044-2968 Founded in 1877 by Paul Groth Zeitschrift für Kristallographie is one of the world’s oldest scientific journals. In original papers, letters and review articles it presents results of theoretical or experimental study on crystallography.