{"title":"水热反应大规模合成Sb2S3尖晶","authors":"C. Pilapong, T. Thongtem, S. Thongtem","doi":"10.1109/INEC.2010.5425105","DOIUrl":null,"url":null,"abstract":"Spikes of Sb<inf>2</inf>S<inf>3</inf> (antimony sulfide) were synthesized by hydrothermal reaction at 100–200 °C for 6–48 h. By using X-ray diffraction (XRD), selected area electron diffraction (SAED), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), high resolution TEM (HRTEM) and UV-vis absorption spectroscopy, the products were specified as orthorhombic Sb<inf>2</inf>S<inf>3</inf> in the shape of spikes, with their growths in the [001] direction and E<inf>g</inf> of 5.40 eV. A diffraction pattern was also simulated, and was in good accordance with the SAED pattern obtained from the experiment.","PeriodicalId":6390,"journal":{"name":"2010 3rd International Nanoelectronics Conference (INEC)","volume":"53 1","pages":"558-559"},"PeriodicalIF":0.0000,"publicationDate":"2010-03-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Large-scale synthesis of Sb2S3 spikes by hydrothermal reaction\",\"authors\":\"C. Pilapong, T. Thongtem, S. Thongtem\",\"doi\":\"10.1109/INEC.2010.5425105\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Spikes of Sb<inf>2</inf>S<inf>3</inf> (antimony sulfide) were synthesized by hydrothermal reaction at 100–200 °C for 6–48 h. By using X-ray diffraction (XRD), selected area electron diffraction (SAED), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), high resolution TEM (HRTEM) and UV-vis absorption spectroscopy, the products were specified as orthorhombic Sb<inf>2</inf>S<inf>3</inf> in the shape of spikes, with their growths in the [001] direction and E<inf>g</inf> of 5.40 eV. A diffraction pattern was also simulated, and was in good accordance with the SAED pattern obtained from the experiment.\",\"PeriodicalId\":6390,\"journal\":{\"name\":\"2010 3rd International Nanoelectronics Conference (INEC)\",\"volume\":\"53 1\",\"pages\":\"558-559\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2010-03-04\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"2010 3rd International Nanoelectronics Conference (INEC)\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1109/INEC.2010.5425105\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"2010 3rd International Nanoelectronics Conference (INEC)","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1109/INEC.2010.5425105","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Large-scale synthesis of Sb2S3 spikes by hydrothermal reaction
Spikes of Sb2S3 (antimony sulfide) were synthesized by hydrothermal reaction at 100–200 °C for 6–48 h. By using X-ray diffraction (XRD), selected area electron diffraction (SAED), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), high resolution TEM (HRTEM) and UV-vis absorption spectroscopy, the products were specified as orthorhombic Sb2S3 in the shape of spikes, with their growths in the [001] direction and Eg of 5.40 eV. A diffraction pattern was also simulated, and was in good accordance with the SAED pattern obtained from the experiment.
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