不同制备方法对(YBCO)超导体化合物组成及介电性能的影响

Haider M. J. Haider, K. Jasim
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引用次数: 8

摘要

采用固态反应(SSR)、溶胶-凝胶(SG)和激光脉冲沉积(PLD)法制备了超导体化合物YBa2Cu2.8Zn0.2O7+δ。采用x射线衍射技术,所有样品均呈正交晶系,高相(Y-123)增加,低相(Y-123)减少,并随制备方法的不同而呈比例变化,出现一些杂质。对样品的电阻和临界温度进行了研究,发现样品均表现出超导行为。研究了室温下介电常数(实介电常数、虚介电常数、损耗正切、交变电导率)随频率和范围(50 Hz-1MHz)的变化规律。研究结果表明,采用激光脉冲沉积法制备PLD后,其介电性能发生了明显的变化,并通过扫描电子显微镜(SEM)对样品进行了高量级的显微成像。另外用滴定法测定氧的比例。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Effect of Composition and Dielectric Properties for (YBCO) Superconductor Compound in Different Preparation Methods
The superconductor compound (YBa2Cu2.8Zn0.2O7+δ) is prepared by solid state reaction (SSR), Sol-gel (SG) and laser Pulse deposition (PLD) methods. We used the X-ray diffraction technique, which shows an orthorhombic crystalline system for all the samples, and increase in the high-phase (Y-123) and decrease in low-phase and vary in proportion according to the method of preparation with the emergence of some impurities. The behavior of the samples in terms of electrical resistance and critical temperature was investigated all samples showed superconducting behavior. The properties of the dielectric (real dielectric constant, imaginary dielectric constant, loss tangent, alternating electrical conductivity) were studied as a function of frequency and range (50 Hz-1MHz) at room temperature. The results are demonstrate the apparent change in the dielectric properties by using the method of preparation of laser pulse deposition PLD at the expense of other methods, Microscopic images of the samples were examined at very high magnitudes through the scanning electron microscopy (SEM). In addition to using the titration method to determine the proportion of oxygen.
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