NaOH助剂水解TiCl4制备TiO2纳米结构及表征

Al-Mustansiriyah Journal of Sciences Pub Date : 2018-04-11 DOI:10.23851/MJS.V28I2.506

R. Rasheed

{"title":"NaOH助剂水解TiCl4制备TiO2纳米结构及表征","authors":"R. Rasheed","doi":"10.23851/MJS.V28I2.506","DOIUrl":null,"url":null,"abstract":"Titanium dioxide (TiO2) nanostructures were synthesized via the hydrolysis of TiCl4 in alcohol / water solution/with sodium hydroxide solution in the ice-bath (0-5 ◦C). The particles were char-acterized by using X-ray diffraction technique (XRD), spectroscopy of Ultra Violet-Visible (UV / Visible) and infrared (FT-IR), atomic force microscope (AFM) and scanning electron micro-scope (SEM) analysis were used in order to gain information about the material, morphology, size and the shape of the particles","PeriodicalId":7515,"journal":{"name":"Al-Mustansiriyah Journal of Sciences","volume":"32 1","pages":"100-107"},"PeriodicalIF":0.0000,"publicationDate":"2018-04-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"3","resultStr":"{\"title\":\"Preparation and Characterization of TiO2 Nanostructure by TiCl4 Hydrolysis with Additive NaOH\",\"authors\":\"R. Rasheed\",\"doi\":\"10.23851/MJS.V28I2.506\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Titanium dioxide (TiO2) nanostructures were synthesized via the hydrolysis of TiCl4 in alcohol / water solution/with sodium hydroxide solution in the ice-bath (0-5 ◦C). The particles were char-acterized by using X-ray diffraction technique (XRD), spectroscopy of Ultra Violet-Visible (UV / Visible) and infrared (FT-IR), atomic force microscope (AFM) and scanning electron micro-scope (SEM) analysis were used in order to gain information about the material, morphology, size and the shape of the particles\",\"PeriodicalId\":7515,\"journal\":{\"name\":\"Al-Mustansiriyah Journal of Sciences\",\"volume\":\"32 1\",\"pages\":\"100-107\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2018-04-11\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"3\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Al-Mustansiriyah Journal of Sciences\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.23851/MJS.V28I2.506\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Al-Mustansiriyah Journal of Sciences","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.23851/MJS.V28I2.506","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}

引用次数: 3

摘要

在0-5℃冰浴中，采用乙醇/水溶液/氢氧化钠溶液水解二氧化钛(TiO2)纳米结构。采用x射线衍射技术(XRD)、紫外可见光谱(UV / Visible)和红外光谱(FT-IR)、原子力显微镜(AFM)和扫描电子显微镜(SEM)对颗粒进行了表征，以获得颗粒的材料、形貌、尺寸和形状等信息

本文章由计算机程序翻译，如有差异，请以英文原文为准。

查看原文本刊更多论文

Preparation and Characterization of TiO2 Nanostructure by TiCl4 Hydrolysis with Additive NaOH

Titanium dioxide (TiO2) nanostructures were synthesized via the hydrolysis of TiCl4 in alcohol / water solution/with sodium hydroxide solution in the ice-bath (0-5 ◦C). The particles were char-acterized by using X-ray diffraction technique (XRD), spectroscopy of Ultra Violet-Visible (UV / Visible) and infrared (FT-IR), atomic force microscope (AFM) and scanning electron micro-scope (SEM) analysis were used in order to gain information about the material, morphology, size and the shape of the particles

求助全文

通过发布文献求助，成功后即可免费获取论文全文。去求助

来源期刊

Al-Mustansiriyah Journal of Sciences

自引率

0.00%

发文量