NaOH助剂水解TiCl4制备TiO2纳米结构及表征

Al-Mustansiriyah Journal of Sciences Pub Date : 2018-04-11 DOI:10.23851/MJS.V28I2.506

R. Rasheed

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引用次数: 3

摘要

在0-5℃冰浴中，采用乙醇/水溶液/氢氧化钠溶液水解二氧化钛(TiO2)纳米结构。采用x射线衍射技术(XRD)、紫外可见光谱(UV / Visible)和红外光谱(FT-IR)、原子力显微镜(AFM)和扫描电子显微镜(SEM)对颗粒进行了表征，以获得颗粒的材料、形貌、尺寸和形状等信息

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Preparation and Characterization of TiO2 Nanostructure by TiCl4 Hydrolysis with Additive NaOH

Titanium dioxide (TiO2) nanostructures were synthesized via the hydrolysis of TiCl4 in alcohol / water solution/with sodium hydroxide solution in the ice-bath (0-5 ◦C). The particles were char-acterized by using X-ray diffraction technique (XRD), spectroscopy of Ultra Violet-Visible (UV / Visible) and infrared (FT-IR), atomic force microscope (AFM) and scanning electron micro-scope (SEM) analysis were used in order to gain information about the material, morphology, size and the shape of the particles

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Al-Mustansiriyah Journal of Sciences

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