不同空气爆破压力对聚醚醚酮(PEEK)表面粗糙度和与胶结树脂水泥结合强度的影响:体外研究

Yasmin ElFiky, Omnia Nabil, H. Alansary
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摘要

问题陈述:聚醚醚酮材料具有良好的物理力学性能,但缺乏与树脂水泥良好粘结强度的最佳空气爆破参数研究。目的:评价不同空气爆破压力对聚醚醚酮(PEEK)表面粗糙度和与树脂水泥的剪切结合强度的影响。材料和方法:制备了24片BioHPP PEEK (bredent, UK)。用110 μm Al 2o3颗粒在10 mm距离处空气爆破10秒,按压力大小分为3组。A组:3bar, B组:2.5 bar, C组:3.5 bar。表面粗糙度通过扫描电镜测量,涂上Visio Link底漆(Bredent, Germany)并固化,然后涂上G-CEM树脂水泥(GC, Japan)并固化。剪切强度采用万能试验机进行测定。进行了EDX分析,并用立体显微镜检测了失效模式。结果:统计学分析显示,粗糙度平均值(Ra)随压力的增加而升高,其中B组最低(p < 0.05),其他组间差异不显著(p > 0.05)。剪切结合强度A组(12.6864±2.486 MPa)、B组(11.2842±1.555 MPa)、C组(10.1024±2.317 MPa), A、C组间差异有统计学意义(p < 0.05)。C组以粘结破坏为主,A组和b组混合破坏。EDX分析表明,粘结强度试验后,碳和硅的重量百分比增加,氧和铝的重量百分比减少。结论:空气爆破压力增加到3bar时,表面粗糙度和树脂水泥的结合强度都有所增加,但超过3bar时,表面粗糙度变差,结合强度下降。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
The effect of different air blasting pressure of polyetheretherketone (PEEK) on surface roughness and bond strength to adhesive resin cement: An in-vitro study
Statement of the Problem: Polyetheretherketone material shows good physical and mechanical properties but research is lacking optimum air blasting parameters for good bond strength to resin cement. Aim: To evaluate the effect of different air blasting pressure of PEEK on surface roughness and shear bond strength to adhesive resin cement. Materials and Methods: 24 discs of BioHPP PEEK (bredent, UK) were manufactured. Samples were air blasted with 110 μm Al 2 O 3 particles for 10 seconds at distance of 10 mm and divided into 3 groups according to pressure. Group A: 3 bar, Group B: 2.5 bar and Group C: 3.5 bar. Surface roughness was measured by SEM, Visio Link primer (Bredent, Germany) was applied and cured then G-CEM resin cement (GC, Japan) was applied and cured. Shear bond strength was measured using universal testing machine. EDX analysis was done, and failure mode was detected by stereo-microscope. Results: Statistical analysis showed that roughness average (Ra) increased by increasing pressure, Group B was significantly the lowest ( p < 0.05), while there was insignificant difference between other groups (P > 0.05). Regarding shear bond strength, Group A recorded (12.6864 ± 2.486 MPa), Group B (11.2842 ± 1.555 MPa) and Group C (10.1024 ± 2.317 MPa), there was significantly statistical difference between Groups A & C ( p < 0.05). The failure mode was mainly adhesive in group C and mixed in groups A & B. EDX analysis showed an increase in Carbon and Silica and a decrease in Oxygen and Aluminum weight percentages after the bond strength test. Conclusion: Increasing the air blasting pressure up to 3 bar increases the surface roughness and bond strength to resin cement, but more than 3 bar showed unfavorable surface roughness and decreased bond strength.
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