双(4-甲氧基苯甲酰亚甲基三对苯二酚-磷μ-碘(二碘氨基磺酸))配合物C30H30HgI3O2P的晶体结构

S. Sabounchei, V. Jodaian, A. Dadrass, Hassan Nemattalab, H. Khavasi
{"title":"双(4-甲氧基苯甲酰亚甲基三对苯二酚-磷μ-碘(二碘氨基磺酸))配合物C30H30HgI3O2P的晶体结构","authors":"S. Sabounchei, V. Jodaian, A. Dadrass, Hassan Nemattalab, H. Khavasi","doi":"10.2116/ANALSCIX.24.X111","DOIUrl":null,"url":null,"abstract":"The crystal structure of a colorless complex of [CH3OC6H4COCH2P(p·tolyl)3]2[Hg2I6] was determined by the X-ray diffraction method. All atoms occupy general positions in the monoclinic space group, P21/n and have the following unit-cell dimensions: a = 11.5933(11)A, b = 22.842(3)A, c = 12.2271(12)A, β = 103.719(8)°, Z = 4 and V = 3145.5(6)A3. The final R value is 0.0582.","PeriodicalId":7796,"journal":{"name":"Analytical Sciences: X-ray Structure Analysis Online","volume":"16 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2008-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Crystal Structure of Bis(4-methoxybenzoylmethylenetriparatolyl-phosphonium μ-Iodo(diiodomercurate)) Complex, C30H30HgI3O2P\",\"authors\":\"S. Sabounchei, V. Jodaian, A. Dadrass, Hassan Nemattalab, H. Khavasi\",\"doi\":\"10.2116/ANALSCIX.24.X111\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The crystal structure of a colorless complex of [CH3OC6H4COCH2P(p·tolyl)3]2[Hg2I6] was determined by the X-ray diffraction method. All atoms occupy general positions in the monoclinic space group, P21/n and have the following unit-cell dimensions: a = 11.5933(11)A, b = 22.842(3)A, c = 12.2271(12)A, β = 103.719(8)°, Z = 4 and V = 3145.5(6)A3. The final R value is 0.0582.\",\"PeriodicalId\":7796,\"journal\":{\"name\":\"Analytical Sciences: X-ray Structure Analysis Online\",\"volume\":\"16 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2008-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Analytical Sciences: X-ray Structure Analysis Online\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.2116/ANALSCIX.24.X111\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Analytical Sciences: X-ray Structure Analysis Online","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.2116/ANALSCIX.24.X111","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0

摘要

用x射线衍射法测定了无色配合物[CH3OC6H4COCH2P(p·托利基)3]2[Hg2I6]的晶体结构。所有原子在单斜空间群P21/n中占据一般位置,具有以下单位胞尺寸:a = 11.5933(11) a, b = 22.842(3) a, c = 12.2271(12) a, β = 103.719(8)°,Z = 4, V = 3145.5(6)A3。最终R值为0.0582。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Crystal Structure of Bis(4-methoxybenzoylmethylenetriparatolyl-phosphonium μ-Iodo(diiodomercurate)) Complex, C30H30HgI3O2P
The crystal structure of a colorless complex of [CH3OC6H4COCH2P(p·tolyl)3]2[Hg2I6] was determined by the X-ray diffraction method. All atoms occupy general positions in the monoclinic space group, P21/n and have the following unit-cell dimensions: a = 11.5933(11)A, b = 22.842(3)A, c = 12.2271(12)A, β = 103.719(8)°, Z = 4 and V = 3145.5(6)A3. The final R value is 0.0582.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信