TiN/TiAl3/Ti2AlN复合材料电阻率的温度依赖性

A. A. Kondakov, A. Karpov, V. Grachev, A. Sytschev
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引用次数: 0

摘要

将多孔TiAl金属间样品在气态氮中过滤燃烧,制备了TiN/TiAl3/Ti2AlN复合材料。燃烧产物的x射线相分析提供的数据计算了各相的重量含量如下:42 wt.% TiN, 35 wt.% TiAl3, 20 wt.% Ti2AlN和3 wt.% TiAl。所合成的含Ti2AlN МАХ相的复合材料具有良好的金属导电性。在真空2·10-3 Pa、温度300-1300 K、恒流条件下,采用标准4点法测量合成材料的比电阻。随着温度的升高,比电阻从0.35到1.25 μΩ·m呈线性增长。随后在以下加热/冷却循环中对该指标的测量表明所得结果完全一致。这表明该材料在所研究的温度范围内具有稳定的电物理性质。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Temperature dependence of TiN/TiAl3/Ti2AlN composite material electric resistivity
The TiN/TiAl3/Ti2AlN composite material was obtained by filtration combustion of the porous TiAl intermetallic samples in gaseous nitrogen. X-ray phase analysis of combustion products provided data to calculate the weight content of each phase as follows: 42 wt.% TiN, 35 wt.% TiAl3, 20 wt.% Ti2AlN and 3 wt.% TiAl. The synthesized composite material containing Ti2AlN МАХ phase features good electrical conductivity of a metallic nature. Specific electrical resistance of the synthesized material was measured by a standard 4-point procedure at constant current in the temperature range 300–1300 K in vacuum 2·10–3 Pa. It was found that specific electrical resistance grows linearly from 0.35 to 1.25 μΩ·m as temperature rises. Subsequent measurements of this indicator at the following heating/cooling cycles demonstrated full agreement of obtained results. This fact indicates that the material has stable electrophysical properties in the investigated temperature range.
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