A. A. Kondakov, A. Karpov, V. Grachev, A. Sytschev
{"title":"TiN/TiAl3/Ti2AlN复合材料电阻率的温度依赖性","authors":"A. A. Kondakov, A. Karpov, V. Grachev, A. Sytschev","doi":"10.17073/1997-308x-2019-3-36-41","DOIUrl":null,"url":null,"abstract":"The TiN/TiAl3/Ti2AlN composite material was obtained by filtration combustion of the porous TiAl intermetallic samples in gaseous nitrogen. X-ray phase analysis of combustion products provided data to calculate the weight content of each phase as follows: 42 wt.% TiN, 35 wt.% TiAl3, 20 wt.% Ti2AlN and 3 wt.% TiAl. The synthesized composite material containing Ti2AlN МАХ phase features good electrical conductivity of a metallic nature. Specific electrical resistance of the synthesized material was measured by a standard 4-point procedure at constant current in the temperature range 300–1300 K in vacuum 2·10–3 Pa. It was found that specific electrical resistance grows linearly from 0.35 to 1.25 μΩ·m as temperature rises. Subsequent measurements of this indicator at the following heating/cooling cycles demonstrated full agreement of obtained results. This fact indicates that the material has stable electrophysical properties in the investigated temperature range.","PeriodicalId":14693,"journal":{"name":"Izvestiya vuzov. Poroshkovaya metallurgiya i funktsional’nye pokrytiya","volume":"4 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2019-09-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Temperature dependence of TiN/TiAl3/Ti2AlN composite material electric resistivity\",\"authors\":\"A. A. Kondakov, A. Karpov, V. Grachev, A. Sytschev\",\"doi\":\"10.17073/1997-308x-2019-3-36-41\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The TiN/TiAl3/Ti2AlN composite material was obtained by filtration combustion of the porous TiAl intermetallic samples in gaseous nitrogen. X-ray phase analysis of combustion products provided data to calculate the weight content of each phase as follows: 42 wt.% TiN, 35 wt.% TiAl3, 20 wt.% Ti2AlN and 3 wt.% TiAl. The synthesized composite material containing Ti2AlN МАХ phase features good electrical conductivity of a metallic nature. Specific electrical resistance of the synthesized material was measured by a standard 4-point procedure at constant current in the temperature range 300–1300 K in vacuum 2·10–3 Pa. It was found that specific electrical resistance grows linearly from 0.35 to 1.25 μΩ·m as temperature rises. Subsequent measurements of this indicator at the following heating/cooling cycles demonstrated full agreement of obtained results. This fact indicates that the material has stable electrophysical properties in the investigated temperature range.\",\"PeriodicalId\":14693,\"journal\":{\"name\":\"Izvestiya vuzov. Poroshkovaya metallurgiya i funktsional’nye pokrytiya\",\"volume\":\"4 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2019-09-26\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Izvestiya vuzov. Poroshkovaya metallurgiya i funktsional’nye pokrytiya\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.17073/1997-308x-2019-3-36-41\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Izvestiya vuzov. Poroshkovaya metallurgiya i funktsional’nye pokrytiya","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.17073/1997-308x-2019-3-36-41","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Temperature dependence of TiN/TiAl3/Ti2AlN composite material electric resistivity
The TiN/TiAl3/Ti2AlN composite material was obtained by filtration combustion of the porous TiAl intermetallic samples in gaseous nitrogen. X-ray phase analysis of combustion products provided data to calculate the weight content of each phase as follows: 42 wt.% TiN, 35 wt.% TiAl3, 20 wt.% Ti2AlN and 3 wt.% TiAl. The synthesized composite material containing Ti2AlN МАХ phase features good electrical conductivity of a metallic nature. Specific electrical resistance of the synthesized material was measured by a standard 4-point procedure at constant current in the temperature range 300–1300 K in vacuum 2·10–3 Pa. It was found that specific electrical resistance grows linearly from 0.35 to 1.25 μΩ·m as temperature rises. Subsequent measurements of this indicator at the following heating/cooling cycles demonstrated full agreement of obtained results. This fact indicates that the material has stable electrophysical properties in the investigated temperature range.