合成和描述物质性质和化学催化剂苯- zno

I. Widihati, M. Manurung, N. G. D. A. Suastuti, N. P. A. J. S. Putri
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引用次数: 0

摘要

使用膨润土作为催化剂已被许多研究报道。粘土的催化活性一般不是很高。因此,使用前必须对粘土进行改性处理。研究了氧化锌(膨润土-氧化锌)改性粘土的合成与表征。研究了氧化锌改性膨润土的理化性质。先浸渍膨润土,再插入氧化锌,形成柱状结构。利用x射线衍射、SEM-EDS、FTIR、亚甲基蓝吸附法和酸碱滴定法对合成的膨润土氧化锌催化剂进行了表征。表征结果表明,ZnO嵌入膨润土并没有增加层间的距离,催化剂变得更加均匀,锌元素的数量有所增加,在3600处出现了吸收带;1600 - 1650;在2900 ~ 2850和450 cm-1区域,确定了膨润土氧化锌的官能团特征,其表面积和酸位分别为46.357 m2/g和5.887 × 1022个位点/g。关键词:膨润土;催化剂;表征;
本文章由计算机程序翻译,如有差异,请以英文原文为准。
SINTESIS DAN KARAKTERISASI SIFAT FISIK DAN KIMIA KATALIS BENTONIT-ZnO
The use of bentonite clay as a catalyst has been reported by many studies. The catalytic activity of clays is generally not very high. Therefore, the clay must be modified before use. Synthesis and characterization of ZnO (Bentonite-ZnO) modified clay was carried out. This study aimed to determine the physical and chemical properties of modified Bentonite with ZnO. Bentonite was dipped first and then intercalated with ZnO which was expected to form pillars. The synthesized Bentonite-ZnO was characterized according to the benefits of Bentonite-ZnO as a catalyst using X-Ray Diffraction, SEM-EDS, FTIR, surface area using Methylene Blue adsorption method, and surface acid sites using an acid-base titration method. The characterization results showed that the intercalation of ZnO into bentonite did not increase the distance between layers, the catalyst became more homogeneous and there was an increase in the number of Zn elements, the appearance of absorption bands in the 3600; 1600 – 1650; 2900-2850 and 450 cm-1 regions which identified the functional group characteristics of Bentonite-ZnO and surface area and acid sites of 46.357 m2/g and 5.887 x 1022 sites/g, respectively. Keywords: bentonite, catalyst, characterization, pillared, ZnO.
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