M. Habibi, K. Barati, Hossein Etedali Habibabadi, R. Harrington, W. Clegg
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引用次数: 0
摘要
合成了标题化合物C14H17NO2，并用x射线晶体学对其结构进行了研究。该化合物通过Aldol缩合得到，晶胞参数为a = 6.6758(9)， b = 11.6866(15)， c = 16.348(2) a, V = 1275.4(3)A3, Z = 4，在正交空间群P212121中结晶。分子间和分子内的C-H - O氢键稳定了晶体结构。
Crystal Structure of 3-(4-(Dimethylamino)benzylidene)pentane-2,4-dione
The title compound (I), C14H17NO2, was synthesized and the structure was investigated by X-ray crystallography. The compound was obtained by an Aldol condensation, and crystallized in the orthorhombic space group P212121 with cell parameters a = 6.6758(9), b = 11.6866(15), c = 16.348(2)A, V = 1275.4(3)A3 and Z = 4. The crystal structure is stabilized by inter and intramolecular C-H…O hydrogen bonds.
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