(Ni0.5Zn0.5Fe2O4/CI/CB)三元复合材料的合成及其微波吸收性能

A. Houbi, A. Zharmenov, Yomen Atassi, Z. Bagasharova, S. Mirzalieva, B. Karibayev
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摘要

本文通过两步法制备了NiZn铁氧体/羰基铁/炭黑三元复合材料(Ni0.5Zn0.5Fe2O4/CI/CB)。首先,以蔗糖为燃料,采用自燃法制备Ni0.5Zn0.5Fe2O4。之后,通过磨球混合CB、CI和Ni0.5Zn0.5Fe2O4继续进行操作。制备了三种不同重量比的Ni0.5Zn0.5Fe2O4/CI/CB(1:1:1, 1:1:2和2:1:1),厚度为2-4-6 mm。采用质量比为40% w/w的石蜡基体分散(Ni0.5Zn0.5Fe2O4/CI/CB)复合材料制备吸附剂。用x射线衍射和红外光谱对样品进行了表征。用扫描电镜研究了粉末的形貌。通过测量8.8-12 GHz频段的微波吸收特性来完成功能表征。微波吸收材料在2.81 ~ 3.20 GHz范围内具有-10 dB以下的宽带宽和3.625 ~ 4.041 kg/m2范围内的合理表面密度。在匹配频率为9.92 GHz、厚度为6 mm时,带宽为3.20 GHz的吸波器反射损耗最小,为-19.4 dB。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis and Microwave Absorption Properties of (Ni0.5Zn0.5Fe2O4/CI/CB) Ternary Composites
In this work, ternary composites of NiZn ferrite/carbonyl iron/carbon black (Ni0.5Zn0.5Fe2O4/CI/CB) were prepared via two stages. Firstly, Ni0.5Zn0.5Fe2O4 was prepared by a self-combustion method using sucrose as a fuel. After that, the operation was continued via mixing CB, CI, and Ni0.5Zn0.5Fe2O4 through grinding balls. Three various weight ratios of Ni0.5Zn0.5Fe2O4/CI/CB (1:1:1, 1:1:2, and 2:1:1) with various thicknesses (2–4–6 mm) were prepared. The absorbers were prepared by dispersing (Ni0.5Zn0.5Fe2O4/CI/CB) composites with a weight ratio within a paraffin wax matrix of 40 % w/w. X-ray diffractometry and FTIR spectroscopy were used in order to characterize the samples. The morphology of the powders was investigated by SEM. The functional characterization was accomplished by measuring the microwave absorption properties in the fre-quency band of 8.8–12 GHz. The microwave absorption materials (MAMs) showed wide bandwidths under –10 dB in the range of 2.81–3.20 GHz and reasonable surface density in the range of 3.625–4.041 kg/m2. The absorber of 3.20 GHz bandwidth had a minimal reflection loss of –19.4 dB at the matching frequency of 9.92 GHz with a thickness of 6 mm.
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