玉米壳灰作为可再生原料生产高附加值硅胶及其应用

A. Ananthi, D. Geetha, P. Ramesh
{"title":"玉米壳灰作为可再生原料生产高附加值硅胶及其应用","authors":"A. Ananthi, D. Geetha, P. Ramesh","doi":"10.7176/cmr/13-3-01","DOIUrl":null,"url":null,"abstract":"Nowadays, silica gels have developed a lot of interest due to their extraordinary properties and their existing and potential applications in science and technology. Silica gel has a lot of applications such as a desiccant, as a preservation tool to control humidity, as an adsorbent, as a catalyst and as a catalyst support. Silica gel is a rigid three-dimensional network of colloidal silica, and is classified as: aquagel, xerogel and aero-gel. Extraction of amorphous silica from Maize Husk Ash (MHA) was carried out in this study. Silica xerogel was produced by dissolving MHA with alkali solution to form sodium silicate solution and lowering the pH to7 by adding hydrochloric acid to form silica aquagel followed by drying to form silica xerogel. The silica xerogel was characterized using SEM, XRD and FTIR techniques. Silica and mineral contents of MHA and xerogel were determined by EDS, X-ray diffraction patterns revealed amorphous nature of extracted silica. Fourier transform infrared (FTIR) data indicates the presence of siloxane and silanol groups. Silica yield from MHA was 56.32% while moisture content was 2.89% and also the SEM presented appropriated morphological characteristics of the best silica. MHA proved to be a potential low cost raw material for the production of silica gel.","PeriodicalId":9724,"journal":{"name":"chemistry and materials research","volume":"32 4 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2021-10-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Maize Husk Ash as a Renewable Source for the Production of Value Added Silica Gel and Its Application\",\"authors\":\"A. Ananthi, D. Geetha, P. Ramesh\",\"doi\":\"10.7176/cmr/13-3-01\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Nowadays, silica gels have developed a lot of interest due to their extraordinary properties and their existing and potential applications in science and technology. Silica gel has a lot of applications such as a desiccant, as a preservation tool to control humidity, as an adsorbent, as a catalyst and as a catalyst support. Silica gel is a rigid three-dimensional network of colloidal silica, and is classified as: aquagel, xerogel and aero-gel. Extraction of amorphous silica from Maize Husk Ash (MHA) was carried out in this study. Silica xerogel was produced by dissolving MHA with alkali solution to form sodium silicate solution and lowering the pH to7 by adding hydrochloric acid to form silica aquagel followed by drying to form silica xerogel. The silica xerogel was characterized using SEM, XRD and FTIR techniques. Silica and mineral contents of MHA and xerogel were determined by EDS, X-ray diffraction patterns revealed amorphous nature of extracted silica. Fourier transform infrared (FTIR) data indicates the presence of siloxane and silanol groups. Silica yield from MHA was 56.32% while moisture content was 2.89% and also the SEM presented appropriated morphological characteristics of the best silica. MHA proved to be a potential low cost raw material for the production of silica gel.\",\"PeriodicalId\":9724,\"journal\":{\"name\":\"chemistry and materials research\",\"volume\":\"32 4 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2021-10-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"chemistry and materials research\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.7176/cmr/13-3-01\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"chemistry and materials research","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.7176/cmr/13-3-01","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0

摘要

目前,硅胶由于其非凡的性能以及在科学和技术方面的现有和潜在应用而引起了人们的广泛关注。硅胶有很多用途,如干燥剂,作为保存工具来控制湿度,作为吸附剂,作为催化剂和催化剂载体。硅胶是一种刚性的三维网状胶体二氧化硅,分为:水凝胶、干凝胶和气凝胶。以玉米壳灰(MHA)为原料,进行了无定形二氧化硅的提取。二氧化硅干凝胶是将MHA与碱溶液溶解形成水玻璃溶液,加入盐酸将pH降至7形成二氧化硅水凝胶,然后干燥形成二氧化硅干凝胶。利用扫描电镜(SEM)、x射线衍射(XRD)和红外光谱(FTIR)等技术对二氧化硅干凝胶进行了表征。能谱仪测定了MHA和干凝胶中二氧化硅和矿物质的含量,x射线衍射图显示了所提取二氧化硅的无定形性质。傅里叶变换红外(FTIR)数据表明存在硅氧烷和硅醇基团。MHA制得的二氧化硅收率为56.32%,含水率为2.89%,扫描电镜也显示出最佳二氧化硅的形态特征。MHA被证明是一种潜在的低成本硅胶原料。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Maize Husk Ash as a Renewable Source for the Production of Value Added Silica Gel and Its Application
Nowadays, silica gels have developed a lot of interest due to their extraordinary properties and their existing and potential applications in science and technology. Silica gel has a lot of applications such as a desiccant, as a preservation tool to control humidity, as an adsorbent, as a catalyst and as a catalyst support. Silica gel is a rigid three-dimensional network of colloidal silica, and is classified as: aquagel, xerogel and aero-gel. Extraction of amorphous silica from Maize Husk Ash (MHA) was carried out in this study. Silica xerogel was produced by dissolving MHA with alkali solution to form sodium silicate solution and lowering the pH to7 by adding hydrochloric acid to form silica aquagel followed by drying to form silica xerogel. The silica xerogel was characterized using SEM, XRD and FTIR techniques. Silica and mineral contents of MHA and xerogel were determined by EDS, X-ray diffraction patterns revealed amorphous nature of extracted silica. Fourier transform infrared (FTIR) data indicates the presence of siloxane and silanol groups. Silica yield from MHA was 56.32% while moisture content was 2.89% and also the SEM presented appropriated morphological characteristics of the best silica. MHA proved to be a potential low cost raw material for the production of silica gel.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信